4-(3-{2-[3-(3-(3-Methyl-butoxy)-5-{2-[4-(5-methyl-[1,2,4]oxadiazol-3-yl)-phenyl]-ethoxy}-phenoxy)-propyl]-phenoxy}-propyl)-phenol

Base Information

Chemical Name:4-(3-{2-[3-(3-(3-Methyl-butoxy)-5-{2-[4-(5-methyl-[1,2,4]oxadiazol-3-yl)-phenyl]-ethoxy}-phenoxy)-propyl]-phenoxy}-propyl)-phenol
CAS No.:215245-09-3
Molecular Formula:C₄₀H₄₆N₂O₆
Molecular Weight:650.815
Hs Code.:

Synonyms:4-(3-{2-[3-(3-(3-Methyl-butoxy)-5-{2-[4-(5-methyl-[1,2,4]oxadiazol-3-yl)-phenyl]-ethoxy}-phenoxy)-propyl]-phenoxy}-propyl)-phenol

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Chemical Property of 4-(3-{2-[3-(3-(3-Methyl-butoxy)-5-{2-[4-(5-methyl-[1,2,4]oxadiazol-3-yl)-phenyl]-ethoxy}-phenoxy)-propyl]-phenoxy}-propyl)-phenol

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Technology Process of 4-(3-{2-[3-(3-(3-Methyl-butoxy)-5-{2-[4-(5-methyl-[1,2,4]oxadiazol-3-yl)-phenyl]-ethoxy}-phenoxy)-propyl]-phenoxy}-propyl)-phenol

There total 17 articles about 4-(3-{2-[3-(3-(3-Methyl-butoxy)-5-{2-[4-(5-methyl-[1,2,4]oxadiazol-3-yl)-phenyl]-ethoxy}-phenoxy)-propyl]-phenoxy}-propyl)-phenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 215245-08-2
5-Methyl-3-[4-(2-{3-(3-methyl-butoxy)-5-[3-(2-{3-[4-(tetrahydro-pyran-2-yloxy)-phenyl]-propoxy}-phenyl)-propoxy]-phenoxy}-ethyl)-phenyl]-[1,2,4]oxadiazole

: 215245-09-3
4-(3-{2-[3-(3-(3-Methyl-butoxy)-5-{2-[4-(5-methyl-[1,2,4]oxadiazol-3-yl)-phenyl]-ethoxy}-phenoxy)-propyl]-phenoxy}-propyl)-phenol

Guidance literature:: With Dowex 50WX₂-400; In methanol; toluene; for 0.5h; Ambient temperature;
DOI:10.1016/S0040-4039(98)01657-8

Reference yield:

: 61440-45-7
3-[4-(benzyloxy)phenyl]propan-1-ol

: 215245-09-3
4-(3-{2-[3-(3-(3-Methyl-butoxy)-5-{2-[4-(5-methyl-[1,2,4]oxadiazol-3-yl)-phenyl]-ethoxy}-phenoxy)-propyl]-phenoxy}-propyl)-phenol

Guidance literature:: Multi-step reaction with 7 steps

1: 93 percent / CBr₄, PPh₃ / tetrahydrofuran / 15 h / from 0 deg C to RT

2: 82 percent / NaH / dimethylformamide / 2 h / from 0 deg C to RT

3: 91 percent / CBr₄, PPh₃ / tetrahydrofuran / 15 h / from 0 deg C to RT

4: 82 percent / H₂ / Pd-C / ethyl acetate / 3.5 h / Ambient temperature

5: 86 percent / PPTS / CH₂Cl₂ / 1 h / from 0 deg C to RT

6: 78 percent / NaH / dimethylformamide / 2 h / from 0 deg C to RT

7: 89 percent / Dowex 50WX₂-400 / methanol; toluene / 0.5 h / Ambient temperature

With carbon tetrabromide; Dowex 50WX₂-400; hydrogen; pyridinium p-toluenesulfonate; sodium hydride; triphenylphosphine; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; toluene;
DOI:10.1016/S0040-4039(98)01657-8

Reference yield:

: 10210-17-0
3-(4-hydroxyphenyl)propan-1-ol

: 215245-09-3
4-(3-{2-[3-(3-(3-Methyl-butoxy)-5-{2-[4-(5-methyl-[1,2,4]oxadiazol-3-yl)-phenyl]-ethoxy}-phenoxy)-propyl]-phenoxy}-propyl)-phenol

Guidance literature:: Multi-step reaction with 8 steps

1: 70 percent / NaH / dimethylformamide / 3 h / from 0 deg C to RT

2: 93 percent / CBr₄, PPh₃ / tetrahydrofuran / 15 h / from 0 deg C to RT

3: 82 percent / NaH / dimethylformamide / 2 h / from 0 deg C to RT

4: 91 percent / CBr₄, PPh₃ / tetrahydrofuran / 15 h / from 0 deg C to RT

5: 82 percent / H₂ / Pd-C / ethyl acetate / 3.5 h / Ambient temperature

6: 86 percent / PPTS / CH₂Cl₂ / 1 h / from 0 deg C to RT

7: 78 percent / NaH / dimethylformamide / 2 h / from 0 deg C to RT

8: 89 percent / Dowex 50WX₂-400 / methanol; toluene / 0.5 h / Ambient temperature

With carbon tetrabromide; Dowex 50WX₂-400; hydrogen; pyridinium p-toluenesulfonate; sodium hydride; triphenylphosphine; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; toluene;
DOI:10.1016/S0040-4039(98)01657-8