Naphthalene-2,6-dicarboxylic acid bis-[(2-amino-4,5-dimethyl-phenyl)-methyl-amide]

Base Information

Chemical Name:Naphthalene-2,6-dicarboxylic acid bis-[(2-amino-4,5-dimethyl-phenyl)-methyl-amide]
CAS No.:344881-83-0
Molecular Formula:C₃₀H₃₂N₄O₂
Molecular Weight:480.61
Hs Code.:

Synonyms:Naphthalene-2,6-dicarboxylic acid bis-[(2-amino-4,5-dimethyl-phenyl)-methyl-amide]

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Chemical Property of Naphthalene-2,6-dicarboxylic acid bis-[(2-amino-4,5-dimethyl-phenyl)-methyl-amide]

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Technology Process of Naphthalene-2,6-dicarboxylic acid bis-[(2-amino-4,5-dimethyl-phenyl)-methyl-amide]

There total 3 articles about Naphthalene-2,6-dicarboxylic acid bis-[(2-amino-4,5-dimethyl-phenyl)-methyl-amide] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 344767-39-1
Naphthalene-2,6-dicarboxylic acid bis-[(4,5-dimethyl-2-nitro-phenyl)-methyl-amide]

: 344881-83-0
Naphthalene-2,6-dicarboxylic acid bis-[(2-amino-4,5-dimethyl-phenyl)-methyl-amide]

Guidance literature:: With hydrogen; nickel; In N,N-dimethyl-formamide; at 40 - 70 ℃;

Reference yield:

: 1141-38-4
2,6-Naphthalenedicarboxylic acid

: 344881-83-0
Naphthalene-2,6-dicarboxylic acid bis-[(2-amino-4,5-dimethyl-phenyl)-methyl-amide]

Guidance literature:: Multi-step reaction with 3 steps

1: SOCl₂/pyridine / toluene / 70 - 110 °C

2: N,N-dimethylaniline / toluene / 3 h / Heating

3: H₂ / Raney-Ni / dimethylformamide / 40 - 70 °C

With pyridine; thionyl chloride; hydrogen; N,N-dimethyl-aniline; nickel; In N,N-dimethyl-formamide; toluene;

Reference yield:

: 2351-36-2
2,6-dichloroformyl naphthalene

: 344881-83-0
Naphthalene-2,6-dicarboxylic acid bis-[(2-amino-4,5-dimethyl-phenyl)-methyl-amide]

Guidance literature:: Multi-step reaction with 2 steps

1: N,N-dimethylaniline / toluene / 3 h / Heating

2: H₂ / Raney-Ni / dimethylformamide / 40 - 70 °C

With hydrogen; N,N-dimethyl-aniline; nickel; In N,N-dimethyl-formamide; toluene;