Technology Process of (4S)-4-[(1S)-2-azido-1-benzylethyl]-2,2-dimethyl-1,3-dioxolane
There total 3 articles about (4S)-4-[(1S)-2-azido-1-benzylethyl]-2,2-dimethyl-1,3-dioxolane which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: lithium hexamethyldisilazane; N,N,N,N,N,N-hexamethylphosphoric triamide / tetrahydrofuran
2: triphenylphosphine; diphenyl phosphoryl azide; diethylazodicarboxylate / tetrahydrofuran
With
N,N,N,N,N,N-hexamethylphosphoric triamide; diphenyl phosphoryl azide; triphenylphosphine; lithium hexamethyldisilazane; diethylazodicarboxylate;
In
tetrahydrofuran;
DOI:10.1016/j.bmcl.2014.04.054
- Guidance literature:
-
Multi-step reaction with 3 steps
1: lithium aluminium tetrahydride / tetrahydrofuran
2: toluene-4-sulfonic acid
3: triphenylphosphine; diethylazodicarboxylate; diphenyl phosphoryl azide / tetrahydrofuran
With
lithium aluminium tetrahydride; diphenyl phosphoryl azide; toluene-4-sulfonic acid; triphenylphosphine; diethylazodicarboxylate;
In
tetrahydrofuran;
DOI:10.1016/j.bmcl.2014.04.054
- Guidance literature:
-
Multi-step reaction with 2 steps
1: toluene-4-sulfonic acid
2: triphenylphosphine; diethylazodicarboxylate; diphenyl phosphoryl azide / tetrahydrofuran
With
diphenyl phosphoryl azide; toluene-4-sulfonic acid; triphenylphosphine; diethylazodicarboxylate;
In
tetrahydrofuran;
DOI:10.1016/j.bmcl.2014.04.054
