Technology Process of (2S)-3-azido-2-benzyl-propanal
There total 5 articles about (2S)-3-azido-2-benzyl-propanal which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
periodic acid;
In
tetrahydrofuran; diethyl ether;
for 5h;
DOI:10.1021/jm701049p
- Guidance literature:
-
Multi-step reaction with 5 steps
1: lithium hexamethyldisilazane; N,N,N,N,N,N-hexamethylphosphoric triamide / tetrahydrofuran
2: lithium aluminium tetrahydride / tetrahydrofuran
3: toluene-4-sulfonic acid
4: triphenylphosphine; diethylazodicarboxylate; diphenyl phosphoryl azide / tetrahydrofuran
5: periodic acid / diethyl ether
With
N,N,N,N,N,N-hexamethylphosphoric triamide; lithium aluminium tetrahydride; diphenyl phosphoryl azide; toluene-4-sulfonic acid; periodic acid; triphenylphosphine; lithium hexamethyldisilazane; diethylazodicarboxylate;
In
tetrahydrofuran; diethyl ether;
DOI:10.1016/j.bmcl.2014.04.054
- Guidance literature:
-
Multi-step reaction with 2 steps
1: triphenylphosphine; diethylazodicarboxylate; diphenyl phosphoryl azide / tetrahydrofuran
2: periodic acid / diethyl ether
With
diphenyl phosphoryl azide; periodic acid; triphenylphosphine; diethylazodicarboxylate;
In
tetrahydrofuran; diethyl ether;
DOI:10.1016/j.bmcl.2014.04.054
![(4S)-4-[(1S)-2-azido-1-benzylethyl]-2,2-dimethyl-1,3-dioxolane](/Databaselist/images/loading.webp)
