tetra(4-formylphenoxy)-(2,2'-dihydroxybiphenyl)-cyclo(triphosphazene)

Base Information

Chemical Name:tetra(4-formylphenoxy)-(2,2'-dihydroxybiphenyl)-cyclo(triphosphazene)
CAS No.:1046802-60-1
Molecular Formula:C₄₀H₂₈N₃O₁₀P₃
Molecular Weight:803.598
Hs Code.:

Synonyms:tetra(4-formylphenoxy)-(2,2'-dihydroxybiphenyl)-cyclo(triphosphazene)

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Chemical Property of tetra(4-formylphenoxy)-(2,2'-dihydroxybiphenyl)-cyclo(triphosphazene)

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Technology Process of tetra(4-formylphenoxy)-(2,2'-dihydroxybiphenyl)-cyclo(triphosphazene)

There total 2 articles about tetra(4-formylphenoxy)-(2,2'-dihydroxybiphenyl)-cyclo(triphosphazene) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 128175-79-1
4',4',6',6'-tetrachloro-4'λ⁵,6λ⁵,6'λ⁵-spiro[dibenzo[d,f][1–3]-dioxaphosphepine-6,2'-[1–6]triazatriphosphinine]

: 22666-84-8
4-hydroxybenzaldehyde sodium salt

: 1046802-60-1
tetra(4-formylphenoxy)-(2,2'-dihydroxybiphenyl)-cyclo(triphosphazene)

Guidance literature:: In tetrahydrofuran; at 20 ℃; for 16h;
DOI:10.1002/chem.200701063

Reference yield: 80.0%

: 940-71-6,16422-79-0
2,2,4,4,6,6-hexachloro-1,3,5-triaza-2,4,6-triphosphorine

: 1806-29-7
2,2'-dihydroxybiphenyl

: 123-08-0,65581-83-1
4-hydroxy-benzaldehyde

: 1046802-60-1
tetra(4-formylphenoxy)-(2,2'-dihydroxybiphenyl)-cyclo(triphosphazene)

Guidance literature:: 2,2,4,4,6,6-hexachloro-1,3,5-triaza-2,4,6-triphosphorine; 2,2'-dihydroxybiphenyl; With potassium carbonate; In tetrahydrofuran; at 0 - 20 ℃; for 2h; Inert atmosphere;

4-hydroxy-benzaldehyde; In tetrahydrofuran; for 48h;
DOI:10.1080/10426507.2011.643434