ethyl (2R,3S)-3-hydroxy-2-(((4-nitrophenyl)sulfonyl)oxy)-3-phenylpropanoate

Base Information

Chemical Name:ethyl (2R,3S)-3-hydroxy-2-(((4-nitrophenyl)sulfonyl)oxy)-3-phenylpropanoate
CAS No.:1116503-88-8
Molecular Formula:C₁₇H₁₇NO₈S
Molecular Weight:395.39
Hs Code.:

Synonyms:ethyl (2R,3S)-3-hydroxy-2-(((4-nitrophenyl)sulfonyl)oxy)-3-phenylpropanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ethyl (2R,3S)-3-hydroxy-2-(((4-nitrophenyl)sulfonyl)oxy)-3-phenylpropanoate

Chemical Property:

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Technology Process of ethyl (2R,3S)-3-hydroxy-2-(((4-nitrophenyl)sulfonyl)oxy)-3-phenylpropanoate

There total 3 articles about ethyl (2R,3S)-3-hydroxy-2-(((4-nitrophenyl)sulfonyl)oxy)-3-phenylpropanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 108741-14-6
(2R,3S)-ethyl 2,3-dihydroxy-3-phenylpropanoate

: 98-74-8
4-Nitrobenzenesulfonyl chloride

: 1116503-88-8
ethyl (2R,3S)-3-hydroxy-2-(((4-nitrophenyl)sulfonyl)oxy)-3-phenylpropanoate

Guidance literature:: With triethylamine; In dichloromethane; at -20 - -10 ℃; for 3h;
DOI:10.1016/j.tet.2018.09.011

Reference yield:

: 4192-77-2
ethyl cinnamate

: 1116503-88-8
ethyl (2R,3S)-3-hydroxy-2-(((4-nitrophenyl)sulfonyl)oxy)-3-phenylpropanoate

Guidance literature:: Multi-step reaction with 2 steps

1: potassium osmate; potassium hexacyanoferrate(III); hydroquinidein 1,4-phthalazinediyl diether; potassium carbonate; methanesulfonamide / water; tert-butyl alcohol / 15 h / 0 °C

2: triethylamine / dichloromethane / 3 h / -20 - -10 °C

With potassium osmate; methanesulfonamide; potassium carbonate; hydroquinidein 1,4-phthalazinediyl diether; triethylamine; potassium hexacyanoferrate(III); In dichloromethane; water; tert-butyl alcohol;
DOI:10.1016/j.tet.2018.09.011

Reference yield:

: 103-36-6
ethyl 3-phenyl-2-propenoate

: 1116503-88-8
ethyl (2R,3S)-3-hydroxy-2-(((4-nitrophenyl)sulfonyl)oxy)-3-phenylpropanoate

Guidance literature:: Multi-step reaction with 2 steps

1: water; methanesulfonamide; AD-mix α / tert-butyl alcohol / 16 h / 0 - 20 °C

2: triethylamine / dichloromethane / 1 h / 0 °C

With methanesulfonamide; AD-mix α; water; triethylamine; In dichloromethane; tert-butyl alcohol;