5-(2-Oxo-1,2-dihydro-quinolin-6-yloxy)-pentanoic acid cyclohexyl-methyl-amide

Base Information

Chemical Name:5-(2-Oxo-1,2-dihydro-quinolin-6-yloxy)-pentanoic acid cyclohexyl-methyl-amide
CAS No.:97546-53-7
Molecular Formula:C₂₁H₂₈N₂O₃
Molecular Weight:356.465
Hs Code.:

Synonyms:5-(2-Oxo-1,2-dihydro-quinolin-6-yloxy)-pentanoic acid cyclohexyl-methyl-amide

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Chemical Property of 5-(2-Oxo-1,2-dihydro-quinolin-6-yloxy)-pentanoic acid cyclohexyl-methyl-amide

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Technology Process of 5-(2-Oxo-1,2-dihydro-quinolin-6-yloxy)-pentanoic acid cyclohexyl-methyl-amide

There total 6 articles about 5-(2-Oxo-1,2-dihydro-quinolin-6-yloxy)-pentanoic acid cyclohexyl-methyl-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 100-60-7
N-methylcyclohexylamine

: 62969-53-3
6-(4-carboxybutoxy)carbostyril

: 97546-53-7
5-(2-Oxo-1,2-dihydro-quinolin-6-yloxy)-pentanoic acid cyclohexyl-methyl-amide

Guidance literature:: With triethylamine; isobutyl chloroformate; In N,N-dimethyl-formamide; at 0 ℃; for 0.25h;

Reference yield:

: 14660-52-7
ethyl 5-bromovalerate

: 97546-53-7
5-(2-Oxo-1,2-dihydro-quinolin-6-yloxy)-pentanoic acid cyclohexyl-methyl-amide

Guidance literature:: Multi-step reaction with 3 steps

1: 59.5 percent / K₂CO₃, KI / dimethylsulfoxide / 24 h / Ambient temperature

2: 72 percent / KOH / methanol / 1 h / Heating

3: 40 percent / isobutyl chloroformiate, triethylamine / dimethylformamide / 0.25 h / 0 °C

With potassium hydroxide; potassium carbonate; triethylamine; potassium iodide; isobutyl chloroformate; In methanol; dimethyl sulfoxide; N,N-dimethyl-formamide;

Reference yield:

: 19315-93-6
6-hydroxy-1H-quinolin-2-one

: 97546-53-7
5-(2-Oxo-1,2-dihydro-quinolin-6-yloxy)-pentanoic acid cyclohexyl-methyl-amide

Guidance literature:: Multi-step reaction with 3 steps

1: 59.5 percent / K₂CO₃, KI / dimethylsulfoxide / 24 h / Ambient temperature

2: 72 percent / KOH / methanol / 1 h / Heating

3: 40 percent / isobutyl chloroformiate, triethylamine / dimethylformamide / 0.25 h / 0 °C

With potassium hydroxide; potassium carbonate; triethylamine; potassium iodide; isobutyl chloroformate; In methanol; dimethyl sulfoxide; N,N-dimethyl-formamide;