Technology Process of C12H17BrN2O3
There total 5 articles about C12H17BrN2O3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
(6-amino-4-bromo-2-methoxyphenyl)iminocarbonic acid-bis-(tert-butyl ester);
With
trifluoroacetic acid;
In
dichloromethane;
at 20 ℃;
With
sodium hydroxide;
In
ethyl acetate;
pH=9;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: tetra-(n-butyl)ammonium iodide; sodium hydroxide / tetrahydrofuran; water / 20 °C
2.1: bromine; sodium acetate / acetic acid / 0.25 h / 20 °C
3.1: dmap / dichloromethane / 20 °C
4.1: platinum on activated charcoal; hydrogen / ethanol / 0.75 h / 750.08 Torr
5.1: trifluoroacetic acid / dichloromethane / 20 °C
5.2: pH 9
With
dmap; platinum on activated charcoal; hydrogen; bromine; sodium acetate; tetra-(n-butyl)ammonium iodide; trifluoroacetic acid; sodium hydroxide;
In
tetrahydrofuran; ethanol; dichloromethane; water; acetic acid;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: dmap / dichloromethane / 20 °C
2.1: platinum on activated charcoal; hydrogen / ethanol / 0.75 h / 750.08 Torr
3.1: trifluoroacetic acid / dichloromethane / 20 °C
3.2: pH 9
With
dmap; platinum on activated charcoal; hydrogen; trifluoroacetic acid;
In
ethanol; dichloromethane;