N-<<5-amino-1-(2,3,5-tri-O-acetyl-β-D-ribofuranosyl)-1H-imidazol-4-yl>carbonyl>-3-<(benzyloxy)-NNO-azoxyl>-L-alanine benzyl ester

Base Information

Chemical Name:N-<<5-amino-1-(2,3,5-tri-O-acetyl-β-D-ribofuranosyl)-1H-imidazol-4-yl>carbonyl>-3-<(benzyloxy)-NNO-azoxyl>-L-alanine benzyl ester
CAS No.:90991-41-6
Molecular Formula:C₃₂H₃₆N₆O₁₂
Molecular Weight:696.671
Hs Code.:

Synonyms:N-<<5-amino-1-(2,3,5-tri-O-acetyl-β-D-ribofuranosyl)-1H-imidazol-4-yl>carbonyl>-3-<(benzyloxy)-NNO-azoxyl>-L-alanine benzyl ester

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Chemical Property of N-<<5-amino-1-(2,3,5-tri-O-acetyl-β-D-ribofuranosyl)-1H-imidazol-4-yl>carbonyl>-3-<(benzyloxy)-NNO-azoxyl>-L-alanine benzyl ester

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Technology Process of N-<<5-amino-1-(2,3,5-tri-O-acetyl-β-D-ribofuranosyl)-1H-imidazol-4-yl>carbonyl>-3-<(benzyloxy)-NNO-azoxyl>-L-alanine benzyl ester

There total 3 articles about N-<<5-amino-1-(2,3,5-tri-O-acetyl-β-D-ribofuranosyl)-1H-imidazol-4-yl>carbonyl>-3-<(benzyloxy)-NNO-azoxyl>-L-alanine benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 31.3%

: 90991-39-2
3-<(benzyloxy)-NNO-azoxy>-L-alanine benzyl ester hydrochloride

: 53459-70-4
N-[5-amino-1-(tri-O-acetyl-β-D-ribofuranosyl)-1H-imidazole-4-carbonyloxy]-succinimide

: 90991-41-6
N-<<5-amino-1-(2,3,5-tri-O-acetyl-β-D-ribofuranosyl)-1H-imidazol-4-yl>carbonyl>-3-<(benzyloxy)-NNO-azoxyl>-L-alanine benzyl ester

Guidance literature:: With TEA; In dichloromethane; for 120h; Ambient temperature;
DOI:10.1021/jm00376a012

Reference yield:

: 100-39-0
benzyl bromide

: 90991-41-6
N-<<5-amino-1-(2,3,5-tri-O-acetyl-β-D-ribofuranosyl)-1H-imidazol-4-yl>carbonyl>-3-<(benzyloxy)-NNO-azoxyl>-L-alanine benzyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 46.2 percent / TEA / ethyl acetate / 120 h / Ambient temperature

2: 53.5 percent / HCl / acetic acid / 4.5 h

3: 31.3 percent / TEA / CH₂Cl₂ / 120 h / Ambient temperature

With hydrogenchloride; TEA; In dichloromethane; acetic acid; ethyl acetate;
DOI:10.1021/jm00376a012

Reference yield:

: 90991-37-0
N-(benzyloxycarbonyl)-3-<(benzyloxy)-NNO-azoxy>-L-alanine benzyl ester

: 90991-41-6
N-<<5-amino-1-(2,3,5-tri-O-acetyl-β-D-ribofuranosyl)-1H-imidazol-4-yl>carbonyl>-3-<(benzyloxy)-NNO-azoxyl>-L-alanine benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 53.5 percent / HCl / acetic acid / 4.5 h

2: 31.3 percent / TEA / CH₂Cl₂ / 120 h / Ambient temperature

With hydrogenchloride; TEA; In dichloromethane; acetic acid;
DOI:10.1021/jm00376a012