C₂₈H₃₉N₉O₃

Base Information

Chemical Name:C₂₈H₃₉N₉O₃
CAS No.:1427038-82-1
Molecular Formula:C₂₈H₃₉N₉O₃
Molecular Weight:549.676
Hs Code.:

C<sub>28</sub>H<sub>39</sub>N<sub>9</sub>O<sub>3</sub>

Synonyms:C₂₈H₃₉N₉O₃

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Chemical Property of C₂₈H₃₉N₉O₃

Chemical Property:

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Technology Process of C₂₈H₃₉N₉O₃

There total 8 articles about C₂₈H₃₉N₉O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 931-15-7,931-16-8,6850-38-0,6982-39-4,33092-82-9,38898-70-3,74111-21-0,108267-20-5
(1S,2S)-trans-2-aminocyclohexanol

: 1427038-82-1
C₂₈H₃₉N₉O₃

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium carbonate; acetic anhydride / water; acetone / 3 h / 0 - 20 °C

1.2: 3 h / 0 - 20 °C

1.3: 1 h / Reflux; Enzymatic reaction

2.1: sodium hydroxide / water; 1,4-dioxane / 0 °C

3.1: triethylamine / dichloromethane / 0 h / 0 °C / Inert atmosphere

4.1: sodium azide / N,N-dimethyl-formamide / 55 °C / Inert atmosphere

5.1: trifluoroacetic acid / 0.5 h / Inert atmosphere

5.2: 2 h / 4 °C / Inert atmosphere

6.1: N-ethyl-N,N-diisopropylamine / acetonitrile / 2 h

With sodium azide; acetic anhydride; sodium carbonate; triethylamine; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; sodium hydroxide; In 1,4-dioxane; dichloromethane; water; N,N-dimethyl-formamide; acetone; acetonitrile;
DOI:10.1021/ja401151v

Reference yield:

: 118457-61-7
(1S,2S)-2-azido-1-(trimethylsilyloxy)cyclohexane

: 1427038-82-1
C₂₈H₃₉N₉O₃

Guidance literature:: Multi-step reaction with 7 steps

1.1: trifluoroacetic acid; platinum(IV) oxide; hydrogen / methanol / 40.5 h / 20 °C

2.1: sodium carbonate; acetic anhydride / water; acetone / 3 h / 0 - 20 °C

2.2: 3 h / 0 - 20 °C

2.3: 1 h / Reflux; Enzymatic reaction

3.1: sodium hydroxide / water; 1,4-dioxane / 0 °C

4.1: triethylamine / dichloromethane / 0 h / 0 °C / Inert atmosphere

5.1: sodium azide / N,N-dimethyl-formamide / 55 °C / Inert atmosphere

6.1: trifluoroacetic acid / 0.5 h / Inert atmosphere

6.2: 2 h / 4 °C / Inert atmosphere

7.1: N-ethyl-N,N-diisopropylamine / acetonitrile / 2 h

With platinum(IV) oxide; sodium azide; hydrogen; acetic anhydride; sodium carbonate; triethylamine; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; sodium hydroxide; In 1,4-dioxane; methanol; dichloromethane; water; N,N-dimethyl-formamide; acetone; acetonitrile;
DOI:10.1021/ja401151v

Reference yield:

: 260065-86-9
(1R,2S)-2-amino-1-cyclohexanol

: 1427038-82-1
C₂₈H₃₉N₉O₃

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium hydroxide / water; 1,4-dioxane / 0 °C

2.1: triethylamine / dichloromethane / 0 h / 0 °C / Inert atmosphere

3.1: sodium azide / N,N-dimethyl-formamide / 55 °C / Inert atmosphere

4.1: trifluoroacetic acid / 0.5 h / Inert atmosphere

4.2: 2 h / 4 °C / Inert atmosphere

5.1: N-ethyl-N,N-diisopropylamine / acetonitrile / 2 h

With sodium azide; triethylamine; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; sodium hydroxide; In 1,4-dioxane; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/ja401151v