2,6-dichloro-4-cyano-N-(3,5-difluoropyridin-4-yl)-benzimidoyl chloride

Base Information

Chemical Name:2,6-dichloro-4-cyano-N-(3,5-difluoropyridin-4-yl)-benzimidoyl chloride
CAS No.:1365992-65-9
Molecular Formula:C₁₃H₄Cl₃F₂N₃
Molecular Weight:346.551
Hs Code.:

Synonyms:2,6-dichloro-4-cyano-N-(3,5-difluoropyridin-4-yl)-benzimidoyl chloride

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Chemical Property of 2,6-dichloro-4-cyano-N-(3,5-difluoropyridin-4-yl)-benzimidoyl chloride

Chemical Property:

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Technology Process of 2,6-dichloro-4-cyano-N-(3,5-difluoropyridin-4-yl)-benzimidoyl chloride

There total 3 articles about 2,6-dichloro-4-cyano-N-(3,5-difluoropyridin-4-yl)-benzimidoyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1365992-64-8
2,6-dichloro-4-cyano-N-(3,5-difluoropyridin-4-yl)-benzamide

: 1365992-65-9
2,6-dichloro-4-cyano-N-(3,5-difluoropyridin-4-yl)-benzimidoyl chloride

Guidance literature:: With thionyl chloride; at 80 - 85 ℃; for 61h; Inert atmosphere;

Reference yield:

: 159783-22-9
3,5-difluoropyridin-4-ylamine

: 1365992-65-9
2,6-dichloro-4-cyano-N-(3,5-difluoropyridin-4-yl)-benzimidoyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / N,N-dimethyl-formamide / 0 °C / Inert atmosphere

1.2: 10 °C / Inert atmosphere

2.1: thionyl chloride / 61 h / 80 - 85 °C / Inert atmosphere

With thionyl chloride; sodium hydride; In N,N-dimethyl-formamide;

Reference yield:

: 1258298-06-4
2,6-dichloro-4-cyanobenzoyl chloride

: 1365992-65-9
2,6-dichloro-4-cyano-N-(3,5-difluoropyridin-4-yl)-benzimidoyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / N,N-dimethyl-formamide / 0 °C / Inert atmosphere

1.2: 10 °C / Inert atmosphere

2.1: thionyl chloride / 61 h / 80 - 85 °C / Inert atmosphere

With thionyl chloride; sodium hydride; In N,N-dimethyl-formamide;