trans-4-([(2Z)-3-carboxyprop-2-enoyl]aminolmethyl)cyclohexanecarboxylic acid

Base Information

• Chemical Name: trans-4-([(2Z)-3-carboxyprop-2-enoyl]aminolmethyl)cyclohexanecarboxylic acid
• CAS No.: 69907-68-2
• Molecular Formula: C₁₂H₁₇NO₅
• Molecular Weight: 255.271

Synonyms:trans-4-([(2Z)-3-carboxyprop-2-enoyl]aminolmethyl)cyclohexanecarboxylic acid

Chemical Property of trans-4-([(2Z)-3-carboxyprop-2-enoyl]aminolmethyl)cyclohexanecarboxylic acid

Chemical Property:

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Technology Process of trans-4-([(2Z)-3-carboxyprop-2-enoyl]aminolmethyl)cyclohexanecarboxylic acid

There total 2 articles about trans-4-([(2Z)-3-carboxyprop-2-enoyl]aminolmethyl)cyclohexanecarboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

maleic anhydride (108-31-6) + trans-4-aminomethyl-cyclohexyl-carboxylic acid (1197-18-8) → trans-4-([(2Z)-3-carboxyprop-2-enoyl]aminolmethyl)cyclohexanecarboxylic acid (69907-68-2)

Guidance literature:

In acetonitrile; at 20 ℃; for 6h; Inert atmosphere;

DOI:10.1021/jo201686e

Reference yield:

→ N-(4-Carboxycyclohexylmethyl)-maleinsaeure (69907-68-2,72748-87-9)

Guidance literature:

Maleinsaeureanhydrid, 4-(Aminomethyl)-cyclohexan-1-carbonsaeure;

DOI:10.1111/j.1432-1033.1979.tb19731.x

Reference yield: 94.0%

trans-4-([(2Z)-3-carboxyprop-2-enoyl]aminolmethyl)cyclohexanecarboxylic acid (69907-68-2) + 1-hydroxy-pyrrolidine-2,5-dione (6066-82-6) → trans-2,5-dioxo-1-pyrrolidinyl 4-{[[(2E)-4-[(2,5-dioxo-1-pyrrolidinyl)oxy]-1,4-dioxo-2-buten-1-yl]amino]methyl}tranexamate (1337538-63-2)

Guidance literature:

With pyridine; trifluoroacetic anhydride; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;

DOI:10.1021/jo201686e

upstream raw materials:

maleic anhydride

trans-4-aminomethyl-cyclohexyl-carboxylic acid

Downstream raw materials:

(1r,4r)-4-((2,5-dioxo-2,5-dihydro-1H-pyrrol-1-yl)methyl)cyclohexane-1-carboxylic acid

4-(N-maleimidomethyl)cyclohexanecarboxylic acid N-hydroxysuccinimide ester

C₂₂H₂₉N₃O₇

6-((1r,4r)-4-((2,5-dioxo-2,5-dihydro-1H-pyrrol-1-yl)methyl)cyclohexanecarboxamido)hexanoic acid

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