Technology Process of C29H33FN4O6
There total 10 articles about C29H33FN4O6 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
dmap; triethylamine;
In
ethyl acetate;
at 10 - 15 ℃;
for 0.75h;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: dimethyl sulfoxide / 20 °C
2: 5,5-dimethyl-1,3-cyclohexadiene / 135 °C
3: lithium tert-butoxide / N,N-dimethyl-formamide / 80 °C
4: ethanol / 4.25 h / 0 - 72 °C / Large scale reaction
5: dmap; triethylamine / ethyl acetate / 10 - 15 °C
With
dmap; triethylamine; lithium tert-butoxide;
In
5,5-dimethyl-1,3-cyclohexadiene; ethanol; dimethyl sulfoxide; ethyl acetate; N,N-dimethyl-formamide;
1: Michael condensation;
DOI:10.1021/op100257r
- Guidance literature:
-
Multi-step reaction with 6 steps
1: hydroxylamine / water; isopropyl alcohol / 5.42 h / 58 - 60 °C / Large scale reaction
2: dimethyl sulfoxide / 20 °C
3: 5,5-dimethyl-1,3-cyclohexadiene / 135 °C
4: lithium tert-butoxide / N,N-dimethyl-formamide / 80 °C
5: ethanol / 4.25 h / 0 - 72 °C / Large scale reaction
6: dmap; triethylamine / ethyl acetate / 10 - 15 °C
With
dmap; hydroxylamine; triethylamine; lithium tert-butoxide;
In
5,5-dimethyl-1,3-cyclohexadiene; ethanol; water; dimethyl sulfoxide; ethyl acetate; N,N-dimethyl-formamide; isopropyl alcohol;
2: Michael condensation;
DOI:10.1021/op100257r