N-[(2',3',5'-tri-O-benzoyl-β-D-ribofuranosyl)-carbonyloxy]succinic acid imide

Base Information

Chemical Name:N-[(2',3',5'-tri-O-benzoyl-β-D-ribofuranosyl)-carbonyloxy]succinic acid imide
CAS No.:254440-87-4
Molecular Formula:C₃₁H₂₅NO₁₁
Molecular Weight:587.54
Hs Code.:

Synonyms:N-[(2',3',5'-tri-O-benzoyl-β-D-ribofuranosyl)-carbonyloxy]succinic acid imide

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Chemical Property of N-[(2',3',5'-tri-O-benzoyl-β-D-ribofuranosyl)-carbonyloxy]succinic acid imide

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Technology Process of N-[(2',3',5'-tri-O-benzoyl-β-D-ribofuranosyl)-carbonyloxy]succinic acid imide

There total 3 articles about N-[(2',3',5'-tri-O-benzoyl-β-D-ribofuranosyl)-carbonyloxy]succinic acid imide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 6066-82-6
1-hydroxy-pyrrolidine-2,5-dione

: 23316-68-9
(2R,3R,4R,5R)-3,4-bis(benzoyloxy)-5-((benzoyloxy)methyl)tetrahydrofuran-2-carboxylic acid

: 254440-87-4
N-[(2',3',5'-tri-O-benzoyl-β-D-ribofuranosyl)-carbonyloxy]succinic acid imide

Guidance literature:: With dicyclohexyl-carbodiimide; In 1,2-dichloro-ethane; at 20 ℃; for 24h;

Reference yield:

: 6974-32-9
1-O-acetyl-2,3,5-tri-O-benzoyl-β-D-ribofuranose

: 254440-87-4
N-[(2',3',5'-tri-O-benzoyl-β-D-ribofuranosyl)-carbonyloxy]succinic acid imide

Guidance literature:: Multi-step reaction with 3 steps

1: 79 percent / SnCl₄ / 1,2-dichloro-ethane / 0.03 h

2: 82 percent / HCl; H₂O / acetic acid / 0.25 h / 100 °C

3: DCC / 1,2-dichloro-ethane / 24 h / 25 °C

With hydrogenchloride; water; tin(IV) chloride; dicyclohexyl-carbodiimide; In acetic acid; 1,2-dichloro-ethane; 1: Substitution / 2: Hydrolysis / 3: Substitution;
DOI:10.1039/a905177e

Reference yield:

: 23316-67-8
2,3,5-tri-O-benzoyl-β-D-ribofuranosyl-1-carbonitrile

: 254440-87-4
N-[(2',3',5'-tri-O-benzoyl-β-D-ribofuranosyl)-carbonyloxy]succinic acid imide

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / HCl; H₂O / acetic acid / 0.25 h / 100 °C

2: DCC / 1,2-dichloro-ethane / 24 h / 25 °C

With hydrogenchloride; water; dicyclohexyl-carbodiimide; In acetic acid; 1,2-dichloro-ethane; 1: Hydrolysis / 2: Substitution;
DOI:10.1039/a905177e