[Ni((3,5-di-tert-butylphenyl)2(Ph)(HCC)C₂₀H₈N₄)]

Base Information

Chemical Name:[Ni((3,5-di-tert-butylphenyl)2(Ph)(HCC)C₂₀H₈N₄)]
CAS No.:952190-21-5
Molecular Formula:C₅₆H₅₆N₄Ni
Molecular Weight:843.777
Hs Code.:

[Ni((3,5-di-tert-butylphenyl)2(Ph)(HCC)C<sub>20</sub>H<sub>8</sub>N<sub>4</sub>)]

Synonyms:[Ni((3,5-di-tert-butylphenyl)2(Ph)(HCC)C₂₀H₈N₄)]

Suppliers and Price of [Ni((3,5-di-tert-butylphenyl)2(Ph)(HCC)C₂₀H₈N₄)]

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Chemical Property of [Ni((3,5-di-tert-butylphenyl)2(Ph)(HCC)C₂₀H₈N₄)]

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Technology Process of [Ni((3,5-di-tert-butylphenyl)2(Ph)(HCC)C₂₀H₈N₄)]

There total 1 articles about [Ni((3,5-di-tert-butylphenyl)2(Ph)(HCC)C₂₀H₈N₄)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1075153-52-4
[Ni((3,6-di-tert-butylphenyl)2(Ph)(Me₃SiCC)C₂₀H₈N₄)]

: 952190-21-5
[Ni((3,5-di-tert-butylphenyl)2(Ph)(HCC)C₂₀H₈N₄)]

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; dichloromethane; at 20 ℃; for 0.25h; Inert atmosphere;
DOI:10.1039/c003715j

Reference yield: 91.0%

: 1050506-23-4
mono(trihexylsilyl)acetylene

: 952190-21-5
[Ni((3,5-di-tert-butylphenyl)2(Ph)(HCC)C₂₀H₈N₄)]

: 1244778-18-4
[5,15-bis(3,5-di-tert-butylphenyl)-10-phenyl-20-(trihexylsilylbutadiynyl)porphynato]nickel(II)

Guidance literature:: With CuCl; (CH₃)2NCH₂CH₂N(CH₃)2; air; In tetrahydrofuran; CH₂Cl₂; stirring soln. of porpyrin deriv. and silylacetylene deriv. in CH2Cl2 and THF under dry air, addn. of copper chloride and amine deriv., stirringfor 4 h; filtration through silica, chromy. (silica gel, light petroleum ether/CH2Cl2 (10:1)) under N2, NMR and MS;
DOI:10.1039/c003715j

Reference yield: 83.0%

: 952190-21-5
[Ni((3,5-di-tert-butylphenyl)2(Ph)(HCC)C₂₀H₈N₄)]

: 6919-61-5
N-methoxy-N-methylbenzamide

: 1244778-29-7
[5,15-bis(3,5-di-tert-butylphenyl)-10-phenyl-20-(benzoylethynyl)porphynato]nickel(II)

Guidance literature:: With LiN(Si(CH₃)3)2; In tetrahydrofuran; (inert atm.); addn. of of benzamide deriv. and then lithium amide deriv.in THF to degassed soln. of porpyrin deriv. in THF, stirring at room te mp. for 1 h; addn. of aq. NH4Cl, extn. (CH2Cl2), washing with H2O, chromy. (silica gel, light petroleum ether/CH2Cl2 (4:1)), NMR and MS;
DOI:10.1039/c003715j