N₆-[(4-methoxyphenyl)(diphenyl)methyl]-2',5'-bis-O-[(4-methoxyphenyl)(diphenyl)methyl]adenosine

Base Information

• Chemical Name: N₆-[(4-methoxyphenyl)(diphenyl)methyl]-2',5'-bis-O-[(4-methoxyphenyl)(diphenyl)methyl]adenosine
• CAS No.: 88508-63-8
• Molecular Formula: C₇₀H₆₁N₅O₇
• Molecular Weight: 1084.28

Synonyms:N₆-[(4-methoxyphenyl)(diphenyl)methyl]-2',5'-bis-O-[(4-methoxyphenyl)(diphenyl)methyl]adenosine

Chemical Property of N₆-[(4-methoxyphenyl)(diphenyl)methyl]-2',5'-bis-O-[(4-methoxyphenyl)(diphenyl)methyl]adenosine

Chemical Property:

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Technology Process of N₆-[(4-methoxyphenyl)(diphenyl)methyl]-2',5'-bis-O-[(4-methoxyphenyl)(diphenyl)methyl]adenosine

There total 2 articles about N₆-[(4-methoxyphenyl)(diphenyl)methyl]-2',5'-bis-O-[(4-methoxyphenyl)(diphenyl)methyl]adenosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

mono-4-methoxytrityl chloride (14470-28-1) + adenosine (58-61-7) → (2R,3R,4S,5R)-4-[(4-Methoxy-phenyl)-diphenyl-methoxy]-5-[(4-methoxy-phenyl)-diphenyl-methoxymethyl]-2-(6-{[(4-methoxy-phenyl)-diphenyl-methyl]-amino}-purin-9-yl)-tetrahydro-furan-3-ol (88508-62-7) + N6-[(4-methoxyphenyl)(diphenyl)methyl]-2',5'-bis-O-[(4-methoxyphenyl)(diphenyl)methyl]adenosine (88508-63-8)

Guidance literature:

With pyridine; dmap; at 85 - 88 ℃; for 18h;

DOI:10.1002/jlcr.712

Reference yield: 50.0%

mono-4-methoxytrityl chloride (14470-28-1) + adenosine (58-61-7) → N6-[(4-methoxyphenyl)(diphenyl)methyl]-2',5'-bis-O-[(4-methoxyphenyl)(diphenyl)methyl]adenosine (88508-63-8)

Guidance literature:

With pyridine; at 60 ℃;

DOI:10.1002/cbdv.201000288

Reference yield: 90.0%

trifluoromethylsulfonic anhydride (358-23-6) + N6-[(4-methoxyphenyl)(diphenyl)methyl]-2',5'-bis-O-[(4-methoxyphenyl)(diphenyl)methyl]adenosine (88508-63-8) → Trifluoro-methanesulfonic acid (2R,3R,4R,5R)-4-[(4-methoxy-phenyl)-diphenyl-methoxy]-2-[(4-methoxy-phenyl)-diphenyl-methoxymethyl]-5-(6-{[(4-methoxy-phenyl)-diphenyl-methyl]-amino}-purin-9-yl)-tetrahydro-furan-3-yl ester (667456-01-1)

Guidance literature:

With pyridine; at 0 - 20 ℃; for 0.666667h;

DOI:10.1002/jlcr.712

upstream raw materials:

mono-4-methoxytrityl chloride

adenosine

Downstream raw materials:

Trifluoro-methanesulfonic acid (2R,3R,4R,5R)-4-[(4-methoxy-phenyl)-diphenyl-methoxy]-2-[(4-methoxy-phenyl)-diphenyl-methoxymethyl]-5-(6-{[(4-methoxy-phenyl)-diphenyl-methyl]-amino}-purin-9-yl)-tetrahydro-furan-3-yl ester

(9-{(2R,3S,4S,5R)-4-Fluoro-3-[(4-methoxy-phenyl)-diphenyl-methoxy]-5-[(4-methoxy-phenyl)-diphenyl-methoxymethyl]-tetrahydro-furan-2-yl}-9H-purin-6-yl)-[(4-methoxy-phenyl)-diphenyl-methyl]-amine

N₆-[(4-methoxyphenyl)(diphenyl)methyl]-2',5'-bis-O-[(4-methoxyphenyl)(diphenyl)methyl]-3'-O-[(methylsulfanyl)methyl]-adenosine

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