Phosphonic acid, (acetyloxy)(5-chloro-2-hydroxyphenyl)methyl-, dimethyl ester

Base Information

• Chemical Name: Phosphonic acid, (acetyloxy)(5-chloro-2-hydroxyphenyl)methyl-, dimethyl ester
• CAS No.: 127890-30-6
• Molecular Formula: C₁₁H₁₄ClO₆P
• Molecular Weight: 308.655
• Mol file: 127890-30-6.mol

Synonyms:Phosphonic acid, (acetyloxy)(5-chloro-2-hydroxyphenyl)methyl-, dimethyl ester

Chemical Property of Phosphonic acid, (acetyloxy)(5-chloro-2-hydroxyphenyl)methyl-, dimethyl ester

Chemical Property:

• PSA: 91.87000
• LogP: 3.09320

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Phosphonic acid, (acetyloxy)(5-chloro-2-hydroxyphenyl)methyl-, dimethyl ester

There total 1 articles about Phosphonic acid, (acetyloxy)(5-chloro-2-hydroxyphenyl)methyl-, dimethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 5.0%

Dimethyl phosphite (868-85-9) + 4-chloro-2-formylphenyl acetate (60315-73-3) → 5-chlorosalicyclaldehyde (635-93-8) + Acetic acid (5-chloro-2-hydroxy-phenyl)-(dimethoxy-phosphoryl)-methyl ester (127890-30-6)

Guidance literature:

With 1,4-diaza-bicyclo[2.2.2]octane; In toluene; for 18h; Yields of byproduct given; Ambient temperature;

Reference yield:

acetic anhydride (108-24-7) + Acetic acid (5-chloro-2-hydroxy-phenyl)-(dimethoxy-phosphoryl)-methyl ester (127890-30-6) → dimethyl acetoxy(2-acetoxy-5-chlorophenyl)methylphosphonate

Guidance literature:

With dmap;

upstream raw materials:

Dimethyl phosphite

4-chloro-2-formylphenyl acetate