3,4-Dimethyl-3-cyclohexene-1-carboxylic acid methyl ester

Base Information

Chemical Name:3,4-Dimethyl-3-cyclohexene-1-carboxylic acid methyl ester
CAS No.:5688-48-2
Molecular Formula:C10 H16 O2
Molecular Weight:168.236
Hs Code.:
Mol file:5688-48-2.mol

Synonyms:3,4-Dimethyl-3-cyclohexene-1-carboxylic acid methyl ester;Methyl 3,4-dimethyl-3-cyclohexene-1-carboxylate;Methyl 3,4-dimethyl-3-cyclohexenecarboxylate;

Suppliers and Price of 3,4-Dimethyl-3-cyclohexene-1-carboxylic acid methyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of 3,4-Dimethyl-3-cyclohexene-1-carboxylic acid methyl ester

Chemical Property:

Boiling Point:114 - 116 °C (22 mmHg)
PSA：26.30000
LogP:2.29590

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 3,4-Dimethyl-3-cyclohexene-1-carboxylic acid methyl ester

There total 11 articles about 3,4-Dimethyl-3-cyclohexene-1-carboxylic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 513-81-5
2,3-dimethyl-buta-1,3-diene

: 292638-85-8,9003-21-8,96-33-3
acrylic acid methyl ester

: 5688-48-2,128352-69-2
3,4-dimethyl-cyclohex-3-enecarboxylic acid methyl ester

Guidance literature:: With tert-butylferrocenylmethylsilane; trityl tetrakis(pentafluorophenyl)borate; In dichloromethane; at -78 ℃; Inert atmosphere;
DOI:10.1002/anie.200904520

Reference yield: 95.0%

: ((methyl)2cyclohexenyl)(methoxymethylene)pentacarbonylchromium

: 5688-48-2,128352-69-2
3,4-dimethyl-cyclohex-3-enecarboxylic acid methyl ester

Guidance literature:: With dimethyl sulfoxide; In N,N-dimethyl-formamide; Stirring (35 h, room temp.).; Flash column chromy. (Et2O-CH2Cl2-hexane), (1)H-NMR, IR, MS.;

Reference yield: 91.0%

: ((methyl)2cyclohexenyl)(methoxymethylene)pentacarbonyltungsten

: 5688-48-2,128352-69-2
3,4-dimethyl-cyclohex-3-enecarboxylic acid methyl ester

Guidance literature:: With dimethyl sulfoxide; In N,N-dimethyl-formamide; Stirring (35 h, room temp.).; Flash column chromy. (Et2O-CH2Cl2-hexane).;