Isoxazolo[4,5-d]pyridazin-4(5H)-one, 3,7-dimethyl- (9CI)

Base Information

Chemical Name:Isoxazolo[4,5-d]pyridazin-4(5H)-one, 3,7-dimethyl- (9CI)
CAS No.:129663-22-5
Molecular Formula:C7H7 N3 O2
Molecular Weight:165.151
Hs Code.:
Mol file:129663-22-5.mol

Synonyms:Isoxazolo[4,5-d]pyridazin-4(5H)-one, 3,7-dimethyl- (9CI)

Suppliers and Price of Isoxazolo[4,5-d]pyridazin-4(5H)-one, 3,7-dimethyl- (9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Alichem
3,7-Dimethylisoxazolo[4,5-d]pyridazin-4(5h)-one
1g
$ 562.00

AccelPharmtech
3,7-dimethyl-Isoxazolo[4,5-d]pyridazin-4(5H)-one 97.00%
25G
$ 13300.00

AccelPharmtech
3,7-dimethyl-Isoxazolo[4,5-d]pyridazin-4(5H)-one 97.00%
5G
$ 5360.00

AccelPharmtech
3,7-dimethyl-Isoxazolo[4,5-d]pyridazin-4(5H)-one 97.00%
1G
$ 3120.00

Total 1 raw suppliers

Chemical Property of Isoxazolo[4,5-d]pyridazin-4(5H)-one, 3,7-dimethyl- (9CI)

Chemical Property:

Melting Point:257 °C(Solv: ethanol (64-17-5))
PKA:11.07±0.40(Predicted)
PSA：72.04000
Density:1.58±0.1 g/cm3(Predicted)
LogP:0.94020

Purity/Quality:: 3,7-Dimethylisoxazolo[4,5-d]pyridazin-4(5h)-one ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Isoxazolo[4,5-d]pyridazin-4(5H)-one, 3,7-dimethyl- (9CI)

There total 4 articles about Isoxazolo[4,5-d]pyridazin-4(5H)-one, 3,7-dimethyl- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 129663-13-4
ethyl 5-acetyl-3-methylisoxazole-4-carboxylate

: 129663-22-5
3,7-dimethyl[1,2]oxazolo[4,5-d]pyridazin-4(5H)-one

Guidance literature:: With hydrazine hydrate; In ethanol; for 2h; Reflux;

Reference yield: 82.0%

: 129663-13-4
ethyl 5-acetyl-3-methylisoxazole-4-carboxylate

: 302-01-2,78206-91-4,119775-10-9,75013-58-0
hydrazine

: 129663-22-5
3,7-dimethyl[1,2]oxazolo[4,5-d]pyridazin-4(5H)-one

Guidance literature:: In ethanol; for 2h; Reflux;
DOI:10.1002/jccs.201190076

Reference yield:

: 95104-43-1
5-(1-Hydroxy-ethyl)-3-methyl-isoxazole-4-carboxylic acid ethyl ester

: 129663-22-5
3,7-dimethyl[1,2]oxazolo[4,5-d]pyridazin-4(5H)-one

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / Jones' reagent / acetone / 4 h / Ambient temperature

2: 67 percent / hydrazine hydrate / ethanol / 4 h / Ambient temperature

With jones' reagent; hydrazine hydrate; In ethanol; acetone;