3-Oxa-6,7-diazatricyclo[3.2.2.02,4]non-6-ene, (1-alpha-,2-alpha-,4-alpha-,5-alpha-)- (9CI)

Base Information

Chemical Name:3-Oxa-6,7-diazatricyclo[3.2.2.02,4]non-6-ene, (1-alpha-,2-alpha-,4-alpha-,5-alpha-)- (9CI)
CAS No.:131726-56-2
Molecular Formula:C₆H₈N₂O
Molecular Weight:124.142
Hs Code.:
Mol file:131726-56-2.mol

Synonyms:3-Oxa-6,7-diazatricyclo[3.2.2.02,4]non-6-ene, (1-alpha-,2-alpha-,4-alpha-,5-alpha-)- (9CI)

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Chemical Property of 3-Oxa-6,7-diazatricyclo[3.2.2.02,4]non-6-ene, (1-alpha-,2-alpha-,4-alpha-,5-alpha-)- (9CI)

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Technology Process of 3-Oxa-6,7-diazatricyclo[3.2.2.02,4]non-6-ene, (1-alpha-,2-alpha-,4-alpha-,5-alpha-)- (9CI)

There total 4 articles about 3-Oxa-6,7-diazatricyclo[3.2.2.02,4]non-6-ene, (1-alpha-,2-alpha-,4-alpha-,5-alpha-)- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 131700-10-2
(1R,2R,4S,5S)-3-Oxa-6,7-diaza-tricyclo[3.2.2.0^2,4]non-6-ene 6-oxide

: 131700-09-9,131726-56-2
endo-6,7-diaza-3-oxatricyclo<3.2.2.0^2,4>non-6-ene

Guidance literature:: With hexachlorodisilane; In dichloromethane; for 2h; Heating;
DOI:10.1016/S0040-4039(00)97822-5

Reference yield:

: 78790-57-5
(1R,2R,6S,7S)-4-Methyl-2,4,6-triaza-tricyclo[5.2.2.0^2,6]undec-8-ene-3,5-dione

: 131700-09-9,131726-56-2
endo-6,7-diaza-3-oxatricyclo<3.2.2.0^2,4>non-6-ene

Guidance literature:: Multi-step reaction with 3 steps

1: 90 °C / oxidation under basic conditions

2: 21 percent / m-ClC₆H₄CO₃H / methanol / 72 h / Ambient temperature

3: 76 percent / Si₂Cl₆ / CH₂Cl₂ / 2 h / Heating

With hexachlorodisilane; 3-chloro-benzenecarboperoxoic acid; In methanol; dichloromethane;
DOI:10.1016/S0040-4039(00)97822-5

Reference yield:

: 37436-17-2
2,3-diaza-bicyclo[2.2.2]octa-2,5-diene 2-oxide

: 131700-09-9,131726-56-2
endo-6,7-diaza-3-oxatricyclo<3.2.2.0^2,4>non-6-ene

Guidance literature:: Multi-step reaction with 2 steps

1: 21 percent / m-ClC₆H₄CO₃H / methanol / 72 h / Ambient temperature

2: 76 percent / Si₂Cl₆ / CH₂Cl₂ / 2 h / Heating

With hexachlorodisilane; 3-chloro-benzenecarboperoxoic acid; In methanol; dichloromethane;
DOI:10.1016/S0040-4039(00)97822-5