6,6,7,7,8,8,9,9,10,10,11,11,11-Tridecafluoro-4-iodoundecan-1-ol

Base Information

Chemical Name:6,6,7,7,8,8,9,9,10,10,11,11,11-Tridecafluoro-4-iodoundecan-1-ol
CAS No.:132665-00-0
Molecular Formula:C11H10F13IO
Molecular Weight:532.08
Hs Code.:2905190098
DSSTox Substance ID:DTXSID40446665
Nikkaji Number:J1.309.809C
Mol file:132665-00-0.mol

Synonyms:132665-00-0;6,6,7,7,8,8,9,9,10,10,11,11,11-Tridecafluoro-4-iodoundecan-1-ol;4-Iodo-1H,1H,2H,2H,3H,3H,4H,5H,5H-perfluoroundecan-1-ol;4-Iodo-5-(perfluorohexyl)pentan-1-ol;DTXSID40446665;4-IODO-5-(PERFLUOROHEXYL)PENTAN-1-OL 95%;4-Iodo-6,6,7,7,8,8,9,9,10,10,11,11,11-tridecafluoro-1-undecanol

Suppliers and Price of 6,6,7,7,8,8,9,9,10,10,11,11,11-Tridecafluoro-4-iodoundecan-1-ol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
4-IODO-1H,1H,2H,2H,3H,3H,4H,5H,5H-PERFLUOROUNDECAN-1-OL 95.00%
5MG
$ 498.15

Total 2 raw suppliers

Chemical Property of 6,6,7,7,8,8,9,9,10,10,11,11,11-Tridecafluoro-4-iodoundecan-1-ol

Chemical Property:

Boiling Point:267.7±40.0 °C(Predicted)
PKA:15.00±0.10(Predicted)
PSA：20.23000
Density:1.785±0.06 g/cm3(Predicted)
LogP:5.69140
XLogP3:6.1
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:14
Rotatable Bond Count:9
Exact Mass:531.95688
Heavy Atom Count:26
Complexity:473

Purity/Quality:

97% ^*data from raw suppliers

4-IODO-1H,1H,2H,2H,3H,3H,4H,5H,5H-PERFLUOROUNDECAN-1-OL 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C(CC(CC(C(C(C(C(C(F)(F)F)(F)F)(F)F)(F)F)(F)F)(F)F)I)CO

Technology Process of 6,6,7,7,8,8,9,9,10,10,11,11,11-Tridecafluoro-4-iodoundecan-1-ol

There total 3 articles about 6,6,7,7,8,8,9,9,10,10,11,11,11-Tridecafluoro-4-iodoundecan-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 821-09-0
n-Pent-4-enyl alcohol

: 355-43-1
n-perfluorohexyl iodide

: 132665-00-0
5-(F-hexyl)-4-iodopentanol

Guidance literature:: With 2,2'-azobis(isobutyronitrile); at 80 ℃;
DOI:10.1016/S0022-1139(99)00078-0

Reference yield: 46.0%

: 821-09-0
n-Pent-4-enyl alcohol

: 355-43-1
n-perfluorohexyl iodide

: 132665-00-0
5-(F-hexyl)-4-iodopentanol

: 145193-76-6
5-(F-hexyl)-1,4-diiodopentane

: 135131-52-1
2-(2,2,3,3,4,4,5,5,6,6,7,7,7-tridecafluoroheptyl)-tetrahydrofuran

Guidance literature:: With 2,2'-azobis(isobutyronitrile); at 100 - 110 ℃; for 22h; Yields of byproduct given;
DOI:10.1016/S0022-1139(00)81175-6

Reference yield:

: 3003-84-7
Tetrahydrofurfuryl chloride

: 132665-00-0
5-(F-hexyl)-4-iodopentanol

Guidance literature:: Multi-step reaction with 2 steps

1.1: Na / diethyl ether / 2 h / Heating

1.2: 90 percent / H₂O

2.1: 90 percent / AIBN / 80 °C

With 2,2'-azobis(isobutyronitrile); sodium; In diethyl ether; 1.1: Metallation / 1.2: Hydrolysis / 2.1: Addition;
DOI:10.1016/S0022-1139(99)00078-0