Oxiranemethanol,alpha,3-bis(1-methylethyl)-,[2alpha(S*),3alpha]-(9CI)

Base Information

Chemical Name:Oxiranemethanol,alpha,3-bis(1-methylethyl)-,[2alpha(S*),3alpha]-(9CI)
CAS No.:134175-91-0
Molecular Formula:C9H18O2
Molecular Weight:158.241
Hs Code.:
Mol file:134175-91-0.mol

Synonyms:Oxiranemethanol,alpha,3-bis(1-methylethyl)-,[2alpha(S*),3alpha]-(9CI)

Suppliers and Price of Oxiranemethanol,alpha,3-bis(1-methylethyl)-,[2alpha(S*),3alpha]-(9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of Oxiranemethanol,alpha,3-bis(1-methylethyl)-,[2alpha(S*),3alpha]-(9CI)

Chemical Property:

Boiling Point:216.3±8.0 °C(Predicted)
PKA:14.37±0.20(Predicted)
PSA：32.76000
Density:0.971±0.06 g/cm3(Predicted)
LogP:1.42670

Purity/Quality:: 95% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Oxiranemethanol,alpha,3-bis(1-methylethyl)-,[2alpha(S*),3alpha]-(9CI)

There total 3 articles about Oxiranemethanol,alpha,3-bis(1-methylethyl)-,[2alpha(S*),3alpha]-(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 134111-25-4
1-bromo-1-lithio-2-lithiooxy-3-methylbutane

: 78-84-2
isobutyraldehyde

: 18720-62-2
2-methyl-3-heptanol

: 65429-68-7
5-hydroxy-2,6-dimethyl-heptan-3-one

: 134175-92-1,168399-37-9
(3R*,4S*,5R*)-trans-4,5-epoxy-2,6-dimethyl-3-heptanol

: 134175-91-0,168399-37-9
(3R*,4S*,5R*)-trans-4,5-epoxy-2,6-dimethyl-3-heptanol

Guidance literature:: Yield given. Multistep reaction. Yields of byproduct given;

Reference yield:

: 5923-00-2
2,6-dimethyl-4-heptyn-3-ol

: 134175-91-0,168399-37-9
(3R*,4S*,5R*)-trans-4,5-epoxy-2,6-dimethyl-3-heptanol

Guidance literature:: Multi-step reaction with 2 steps

1: 59 percent / H₂ / Lindlar catalyst / methanol / 2 h / Ambient temperature

2: vanadyl bis(acetylacetonate), tert-butyl hydroperoxide / CH₂Cl₂

With tert.-butylhydroperoxide; bis(acetylacetonate)oxovanadium; hydrogen; Lindlar's catalyst; In methanol; dichloromethane;

Reference yield:

: 134111-21-0
(Z)-2,6-dimethyl-4-hepten-3-ol

: 134175-92-1,168399-37-9
(3R*,4S*,5R*)-trans-4,5-epoxy-2,6-dimethyl-3-heptanol

: 134175-91-0,168399-37-9
(3R*,4S*,5R*)-trans-4,5-epoxy-2,6-dimethyl-3-heptanol

Guidance literature:: With tert.-butylhydroperoxide; bis(acetylacetonate)oxovanadium; In dichloromethane; Title compound not separated from byproducts;