2-(N-Boc-Amino)-3-methylpyridine

Base Information

Chemical Name:2-(N-Boc-Amino)-3-methylpyridine
CAS No.:138343-75-6
Molecular Formula:C11H16N2O2
Molecular Weight:208.26
Hs Code.:2933399090
European Community (EC) Number:628-536-6
ChEMBL ID:CHEMBL4995865
DSSTox Substance ID:DTXSID50471721
Nikkaji Number:J1.056.162K
Wikidata:Q72448267
Mol file:138343-75-6.mol

Synonyms:138343-75-6;2-(N-Boc-Amino)-3-methylpyridine;2-(Boc-amino)-3-methylpyridine;2-BOC-Amino-3-picoline;Tert-butyl N-(3-methylpyridin-2-yl)carbamate;tert-Butyl (3-methylpyridin-2-yl)carbamate;2-tert-butoxycarbonylamino-3-methylpyridine;Carbamic acid, N-(3-methyl-2-pyridinyl)-, 1,1-dimethylethyl ester;MFCD03425358;(3-methyl-pyridin-2-yl)-carbamic acid tert-butyl ester;Carbamic acid, (3-methyl-2-pyridinyl)-, 1,1-dimethylethyl ester;1,1-Dimethylethyl (3-methyl-2-pyridinyl)carbamate;2-(tert-Butoxycarbonylamino)-3-methylpyridine;SCHEMBL68279;CHEMBL4995865;DTXSID50471721;2-(N-Boc)amino-3-methylpyridine;MJPLUXLNYQHWIU-UHFFFAOYSA-N;AKOS004912563;CS-W001433;t-Butyl (3-methyl-2-pyridyl)carbamate;tert-Butyl 3-methyl-2-pyridylcarbamate;2-(Boc-amino)-3-methylpyridine, 97%;10P-376S;4-CYANO-BIPHENYL-4-CARBOXYLICACID;SY028426;2-(t-butoxycarbonylamino)-3-methylpyridine;2-(t-butyloxycarbonylamino)-3-methylpyridine;B6201;FT-0697621;2-(N-t-butoxycarbonylamino)-3-methylpyridine;EN300-176530;TERT-BUTYL 3-METHYLPYRIDIN-2-YLCARBAMATE;A807375;J-506515;Z1505694077;N-(3-methyl-pyridin-2-yl)-carbamic acid tert-butyl ester

Suppliers and Price of 2-(N-Boc-Amino)-3-methylpyridine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
tert-Butyl3-Methylpyridin-2-ylcarbamate
100mg
$ 75.00

Sigma-Aldrich
2-(Boc-amino)-3-methylpyridine 97%
25g
$ 144.00

Matrix Scientific
tert-Butyl(3-methylpyridin-2-yl)carbamate 97%
25g
$ 216.00

Matrix Scientific
tert-Butyl(3-methylpyridin-2-yl)carbamate 97%
50g
$ 360.00

Crysdot
2-(N-Boc-Amino)-3-methylpyridine 97%
100g
$ 286.00

Chemenu
tert-Butyl(3-methylpyridin-2-yl)carbamate 97%
100g
$ 290.00

AOBChem
2-BOC-Amino-3-picoline 95%
100g
$ 271.00

American Custom Chemicals Corporation
2-(BOC-AMINO)-3-METHYLPYRIDINE 95.00%
25G
$ 1209.72

American Custom Chemicals Corporation
2-(BOC-AMINO)-3-METHYLPYRIDINE 95.00%
5G
$ 822.61

Ambeed
2-(N-Boc-Amino)-3-methylpyridine 97%
100g
$ 278.00

Total 28 raw suppliers

Chemical Property of 2-(N-Boc-Amino)-3-methylpyridine

Chemical Property:

Vapor Pressure:0.008mmHg at 25°C
Melting Point:134-138 °C(lit.)
Refractive Index:1.54
Boiling Point:268.5°Cat760mmHg
PKA:12.56±0.70(Predicted)
Flash Point:116.2°C
PSA：51.22000
Density:1.108g/cm³
LogP:2.81000
Storage Temp.:Inert atmosphere,Room Temperature
XLogP3:2.1
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:3
Exact Mass:208.121177757
Heavy Atom Count:15
Complexity:223

Purity/Quality:

99%, ^*data from raw suppliers

tert-Butyl3-Methylpyridin-2-ylcarbamate ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:Xn
Statements: 22-36-43
Safety Statements: 26-36/37

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=C(N=CC=C1)NC(=O)OC(C)(C)C

Technology Process of 2-(N-Boc-Amino)-3-methylpyridine

There total 2 articles about 2-(N-Boc-Amino)-3-methylpyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1603-40-3
3-methylpyridin-2-ylamine

: 24424-99-5
di-tert-butyl dicarbonate

: 138343-75-6
tert-butyl (3-methylpyridin-2-yl)carbamate

Guidance literature:: In tetrahydrofuran; at 60 - 70 ℃; for 3h;
DOI:10.1007/s10870-020-00833-6

Reference yield: 64.0%

: 138343-75-6
tert-butyl (3-methylpyridin-2-yl)carbamate

Guidance literature:

Reference yield: 100.0%

: 138343-75-6
tert-butyl (3-methylpyridin-2-yl)carbamate

: 271-63-6
7-Azaindole

Guidance literature:: tert-butyl (3-methylpyridin-2-yl)carbamate; With n-butyllithium; N,N-dimethyl-formamide; In tetrahydrofuran; at 0 ℃;

With hydrogenchloride; In tetrahydrofuran; water; at 50 ℃;
DOI:10.1021/ol900150u