C-(4-CYCLOPROPYLMETHYL-MORPHOLIN-2-YL)-METHYLAMINE DIHYDROCHLORIDE

Base Information

• Chemical Name: C-(4-CYCLOPROPYLMETHYL-MORPHOLIN-2-YL)-METHYLAMINE DIHYDROCHLORIDE
• CAS No.: 141815-15-8
• Molecular Formula: C₉H₁₈N₂O
• Molecular Weight: 170.255
• Hs Code.: 2934999090
• Mol file: 141815-15-8.mol

Synonyms:C-(4-CYCLOPROPYLMETHYL-MORPHOLIN-2-YL)-METHYLAMINE DIHYDROCHLORIDE

Chemical Property of C-(4-CYCLOPROPYLMETHYL-MORPHOLIN-2-YL)-METHYLAMINE DIHYDROCHLORIDE

Chemical Property:

• PSA: 38.49000
• LogP: 2.29810
• Storage Temp.: Sealed in dry,Room Temperature

Purity/Quality:

97% ^*data from raw suppliers

(4-(cyclopropylmethyl)morpholin-2-yl)methanaminedihydrochloride 95% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of C-(4-CYCLOPROPYLMETHYL-MORPHOLIN-2-YL)-METHYLAMINE DIHYDROCHLORIDE

There total 3 articles about C-(4-CYCLOPROPYLMETHYL-MORPHOLIN-2-YL)-METHYLAMINE DIHYDROCHLORIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-(N-acetylaminomethyl)-4-benzylmorpholine (112913-96-9) → C-(4-Cyclopropylmethyl-morpholin-2-yl)-methylamine (141815-15-8)

Guidance literature:

Multi-step reaction with 3 steps

1: H₂ / 10percent Pd/C / ethanol; acetic acid / 60 °C

2: K₂CO₃, KI / butan-2-one / 17 h / Heating

3: 10percent HCl / 4 h / Heating

With hydrogenchloride; hydrogen; potassium carbonate; potassium iodide; palladium on activated charcoal; In ethanol; acetic acid; butanone;

DOI:10.1248/cpb.40.652

Reference yield:

2-(N-acetylaminomethyl)morpholine (112913-95-8) → C-(4-Cyclopropylmethyl-morpholin-2-yl)-methylamine (141815-15-8)

Guidance literature:

Multi-step reaction with 2 steps

1: K₂CO₃, KI / butan-2-one / 17 h / Heating

2: 10percent HCl / 4 h / Heating

With hydrogenchloride; potassium carbonate; potassium iodide; In butanone;

DOI:10.1248/cpb.40.652

Reference yield:

N-(4-Cyclopropylmethyl-morpholin-2-ylmethyl)-acetamide → C-(4-Cyclopropylmethyl-morpholin-2-yl)-methylamine (141815-15-8)

Guidance literature:

With hydrogenchloride; for 4h; Heating;

DOI:10.1248/cpb.40.652

upstream raw materials:

2-(N-acetylaminomethyl)-4-benzylmorpholine

2-(N-acetylaminomethyl)morpholine

Downstream raw materials:

4-Amino-5-chloro-N-(4-cyclopropylmethyl-morpholin-2-ylmethyl)-2-methoxy-benzamide

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