5-Cyano-4-methyl-6-oxo-1-phenyl-1,6-dihydro-3-pyridazinecarbohydrazide

Base Information

Chemical Name:5-Cyano-4-methyl-6-oxo-1-phenyl-1,6-dihydro-3-pyridazinecarbohydrazide
CAS No.:145121-27-3
Molecular Formula:C13H11 N5 O2
Molecular Weight:269.26
Hs Code.:
Mol file:145121-27-3.mol

Synonyms:5-Cyano-1,6-dihydro-4-methyl-1-phenyl-6-oxopyridazine-3-carboxylicacid hydrazide

Suppliers and Price of 5-Cyano-4-methyl-6-oxo-1-phenyl-1,6-dihydro-3-pyridazinecarbohydrazide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemicals and raw materials
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Total 1 raw suppliers

Chemical Property of 5-Cyano-4-methyl-6-oxo-1-phenyl-1,6-dihydro-3-pyridazinecarbohydrazide

Chemical Property:

PSA：117.29000
LogP:1.29118

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 5-Cyano-4-methyl-6-oxo-1-phenyl-1,6-dihydro-3-pyridazinecarbohydrazide

There total 2 articles about 5-Cyano-4-methyl-6-oxo-1-phenyl-1,6-dihydro-3-pyridazinecarbohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 89516-24-5
ethyl 5-cyano-4-methyl-6-oxo-1-phenyl-1,6-dihydropyridazine-3-carboxylate

: 145121-27-3
5-cyano-4-methyl-1-phenyl-1,6-dihydro-6-oxopyridazine-3-carboxylic acid hydrazide

Guidance literature:: With hydrazine hydrate; In ethanol; for 6h; Heating;

Reference yield:

: 10475-63-5
3-oxo-2-(phenylhydrazono)butyric acid ethyl ester

: 145121-27-3
5-cyano-4-methyl-1-phenyl-1,6-dihydro-6-oxopyridazine-3-carboxylic acid hydrazide

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / AcONH₄ / 0.5 h / 160 °C

2: 70 percent / hydrazine hydrate / ethanol / 0.5 h / Heating

With ammonium acetate; hydrazine hydrate; In ethanol;
DOI:10.1080/10426509808032460