BORON SUB-2 3-NAPHTHALOCYANINE CHLORIDE

Base Information

• Chemical Name: BORON SUB-2 3-NAPHTHALOCYANINE CHLORIDE
• CAS No.: 142710-56-3
• Molecular Formula: C36H18 B Cl N6
• Molecular Weight: 580.843
• Mol file: 142710-56-3.mol

Synonyms:Boron,chloro[8,15:17,24-diimino-26,6-nitrilo-6H-trinaphtho[2,3-c:2',3'-h:2'',3''-m][1,6,11]triazacyclopentadecinato(2-)-N28,N29,N30]-,(T-4)-;8,15:17,24-Diimino-26,6-nitrilo-6H-trinaphtho[2,3-c:2',3'-h:2'',3''-m][1,6,11]triazacyclopentadecine,boron deriv.

Chemical Property of BORON SUB-2 3-NAPHTHALOCYANINE CHLORIDE

Chemical Property:

• Melting Point: 270-276 °C(lit.)
• PSA: 61.42000
• LogP: 8.74410

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of BORON SUB-2 3-NAPHTHALOCYANINE CHLORIDE

There total 4 articles about BORON SUB-2 3-NAPHTHALOCYANINE CHLORIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,3-dicyanonaphthalene (22856-30-0) + boron trichloride (10294-34-5) → boron sub-2,3-naphthalocyanine chloride (142710-56-3) + C36H17BCl2N6 + C36H16BCl3N6 + C36H15BCl4N6

Guidance literature:

In 1,2-dichloro-benzene; at 140 - 180 ℃; for 3.5h;

DOI:10.1039/d1nj03962h

Reference yield:

2,3-dicyanonaphthalene (22856-30-0) + boron trichloride (10294-34-5) → boron sub-2,3-naphthalocyanine chloride (142710-56-3)

Guidance literature:

In further solvent(s); nder N2, ligand suspnd. in solvent, stirred at room temp. with BCl3 (1:4mixt.), heated to 220°C; NMR, UV;

DOI:10.1016/S0277-5387(02)01226-3

Reference yield:

2,3-dicyanonaphthalene (22856-30-0) + boron trichloride (10294-34-5) → boron sub-2,3-naphthalocyanine chloride (142710-56-3) + C36H18BN6(1+) + C36H17BClN6(1+) + C36H17BCl2N6

Guidance literature:

In 1,2-dichloro-benzene; at 180 ℃; for 2h; Solvent; Temperature; Inert atmosphere;

DOI:10.1039/c6ta02457b

upstream raw materials:

2,3-dicyanonaphthalene

boron trichloride

Downstream raw materials:

C₆H₅B((N)NC₁₂H₆)3