3-Buten-2-one, 3-[(acetyloxy)methyl]- (9CI)

Base Information

Chemical Name:3-Buten-2-one, 3-[(acetyloxy)methyl]- (9CI)
CAS No.:152958-65-1
Molecular Formula:C₇H₁₀O₃
Molecular Weight:142.155
Hs Code.:
Mol file:152958-65-1.mol

Synonyms:3-Buten-2-one, 3-[(acetyloxy)methyl]- (9CI)

Suppliers and Price of 3-Buten-2-one, 3-[(acetyloxy)methyl]- (9CI)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-Buten-2-one, 3-[(acetyloxy)methyl]- (9CI)

Chemical Property:

PSA：0.00000
LogP:0.00000

Purity/Quality:

Safty Information:

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Technology Process of 3-Buten-2-one, 3-[(acetyloxy)methyl]- (9CI)

There total 1 articles about 3-Buten-2-one, 3-[(acetyloxy)methyl]- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 73255-29-5
3-(hydroxymethyl)but-3-en-2-one

: 75-36-5
acetyl chloride

: 152958-65-1
acetic acid 2-methylene-3-oxobutyl ester

Guidance literature:: With pyridine; In dichloromethane; at 0 - 23 ℃; for 1.16667h; Inert atmosphere; Autoclave;
DOI:10.1021/jo501004j

Reference yield: 74.0%

: 152958-65-1
acetic acid 2-methylene-3-oxobutyl ester

: 100-52-7
benzaldehyde

: 1613532-93-6
C₁₂H₁₄O₂

Guidance literature:: With dodecacarbonyl-triangulo-triruthenium; carbon monoxide; tetrabutyl-ammonium chloride; water; triethylamine; In 1,4-dioxane; at 75 ℃; for 24h; under 2068.65 Torr; Time; chemoselective reaction; Glovebox; Autoclave;
DOI:10.1021/jo501004j

Reference yield: 73.0%

: 104-53-0
3-phenyl-propionaldehyde

: 152958-65-1
acetic acid 2-methylene-3-oxobutyl ester

: 1613532-95-8
C₁₄H₁₈O₂

Guidance literature:: With dodecacarbonyl-triangulo-triruthenium; carbon monoxide; tetrabutyl-ammonium chloride; water; triethylamine; In 1,4-dioxane; at 75 ℃; for 24h; under 2068.65 Torr; Inert atmosphere;
DOI:10.1021/acs.joc.7b02658