5-Quinoxalinecarbonitrile,1,2,3,4-tetrahydro-6-methyl-2-oxo-(9CI)

Base Information

Chemical Name:5-Quinoxalinecarbonitrile,1,2,3,4-tetrahydro-6-methyl-2-oxo-(9CI)
CAS No.:573692-38-3
Molecular Formula:C10H9N3O
Molecular Weight:187.2
Hs Code.:
Mol file:573692-38-3.mol

Synonyms:5-Quinoxalinecarbonitrile,1,2,3,4-tetrahydro-6-methyl-2-oxo-(9CI);6-METHYL-2-OXO-1,2,3,4-TETRAHYDROQUINOXALINE-5-CARBONITRILE

Suppliers and Price of 5-Quinoxalinecarbonitrile,1,2,3,4-tetrahydro-6-methyl-2-oxo-(9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

AccelPharmtech
1,2,3,4-tetrahydro-6-methyl-2-oxo-5-Quinoxalinecarbonitrile 97.00%
25G
$ 9900.00

Total 2 raw suppliers

Chemical Property of 5-Quinoxalinecarbonitrile,1,2,3,4-tetrahydro-6-methyl-2-oxo-(9CI)

Chemical Property:

Boiling Point:422.5±45.0 °C(Predicted)
PKA:12.95±0.20(Predicted)
PSA：68.41000
Density:1.31±0.1 g/cm3(Predicted)
LogP:1.45378

Purity/Quality:: 1,2,3,4-tetrahydro-6-methyl-2-oxo-5-Quinoxalinecarbonitrile 97.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 5-Quinoxalinecarbonitrile,1,2,3,4-tetrahydro-6-methyl-2-oxo-(9CI)

There total 3 articles about 5-Quinoxalinecarbonitrile,1,2,3,4-tetrahydro-6-methyl-2-oxo-(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (2-cyano-3-methyl-6-nitrophenylamino)acetic acid sodium salt

: 573692-38-3
6-methyl-2-oxo-1,2,3,4-tetrahydroquinoxaline-5-carbonitrile

Guidance literature:: With tin(ll) chloride; In ethanol; for 2h; Heating;
DOI:10.1016/S0968-0896(03)00059-2

Reference yield:

: 6575-09-3
2-chloro-6-methyl-benzonitrile

: 573692-38-3
6-methyl-2-oxo-1,2,3,4-tetrahydroquinoxaline-5-carbonitrile

Guidance literature:: Multi-step reaction with 3 steps

1: 1.61 g / fuming HNO₃; CF₃CO₂H / 20 - 60 °C

2: dimethylformamide / 18 h / 70 °C

3: 149 mg / SnCl₂*2H₂O / ethanol / 2 h / Heating

With nitric acid; trifluoroacetic acid; tin(ll) chloride; In ethanol; N,N-dimethyl-formamide;
DOI:10.1016/S0968-0896(03)00059-2

Reference yield:

: 74671-11-7
2-chloro-6-methyl-3-nitrobenzonitrile

: 573692-38-3
6-methyl-2-oxo-1,2,3,4-tetrahydroquinoxaline-5-carbonitrile

Guidance literature:: Multi-step reaction with 2 steps

1: dimethylformamide / 18 h / 70 °C

2: 149 mg / SnCl₂*2H₂O / ethanol / 2 h / Heating

With tin(ll) chloride; In ethanol; N,N-dimethyl-formamide;
DOI:10.1016/S0968-0896(03)00059-2