2,2-Dibutyl-1,3-dioxolane-4-methanol

Base Information

Chemical Name:2,2-Dibutyl-1,3-dioxolane-4-methanol
CAS No.:5694-78-0
Molecular Formula:C₁₂H₂₄O₃
Molecular Weight:216.321
Hs Code.:
DSSTox Substance ID:DTXSID90972388
Nikkaji Number:J42.138C
Mol file:5694-78-0.mol

Synonyms:2,2-Dibutyl-1,3-dioxolane-4-methanol;5694-78-0;1,3-DIOXOLANE-4-METHANOL, 2,2-DIBUTYL-;(2,2-dibutyl-1,3-dioxolan-4-yl)methanol;DTXSID90972388;LS-62591

Suppliers and Price of 2,2-Dibutyl-1,3-dioxolane-4-methanol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
2,2-DIBUTYL-1,3-DIOXOLANE-4-METHANOL 95.00%
5MG
$ 502.48

Total 3 raw suppliers

Chemical Property of 2,2-Dibutyl-1,3-dioxolane-4-methanol

Chemical Property:

Vapor Pressure:0.000167mmHg at 25°C
Boiling Point:294.7°C at 760 mmHg
Flash Point:144.7°C
PSA：38.69000
Density:0.944g/cm³
LogP:2.47080
XLogP3:2.7
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:7
Exact Mass:216.17254462
Heavy Atom Count:15
Complexity:162

Purity/Quality:: 2,2-DIBUTYL-1,3-DIOXOLANE-4-METHANOL 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCCCC1(OCC(O1)CO)CCCC

Technology Process of 2,2-Dibutyl-1,3-dioxolane-4-methanol

There total 3 articles about 2,2-Dibutyl-1,3-dioxolane-4-methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 98-88-4
benzoyl chloride

: 5694-78-0
(2,2-di-n-butyl-[1,3]dioxolan-4-yl)methanol

: 5694-78-0
(2,2-di-n-butyl-[1,3]dioxolan-4-yl)methanol

: 5694-78-0
(2,2-di-n-butyl-[1,3]dioxolan-4-yl)methanol

: (S)-4-benzoyloxymethyl-2,2-di-n-butyl-1,3-dioxolane

: (R)-4-benzoyloxymethyl-2,2-di-n-butyl-1,3-dioxolane

Guidance literature:: With 4 A molecular sieve; N-ethyl-N,N-diisopropylamine; (S)-1-methyl-2-[(N-benzyl-N-methylamino)methyl]pyrrolidine; In dichloromethane; N,N-dimethyl-formamide; at -78 ℃; for 3h; Title compound not separated from byproducts;
DOI:10.1016/j.tetasy.2005.01.034

Reference yield:

: 98-88-4
benzoyl chloride

: 5694-78-0
(2,2-di-n-butyl-[1,3]dioxolan-4-yl)methanol

: 5694-78-0
(2,2-di-n-butyl-[1,3]dioxolan-4-yl)methanol

: 5694-78-0
(2,2-di-n-butyl-[1,3]dioxolan-4-yl)methanol

: (S)-4-benzoyloxymethyl-2,2-di-n-butyl-1,3-dioxolane

: (R)-4-benzoyloxymethyl-2,2-di-n-butyl-1,3-dioxolane

Guidance literature:: With 4 A molecular sieve; N-ethyl-N,N-diisopropylamine; (S)-1-methyl-2-[(N-benzyl-N-methylamino)methyl]pyrrolidine; In dichloromethane; N,N-dimethyl-formamide; at -78 ℃; for 3h; Title compound not separated from byproducts;
DOI:10.1016/j.tetasy.2005.01.034