p-[2-[(5-Chloro-2-methoxybenzoyl)amino]ethyl]benzenephosphonate

Base Information

• Chemical Name: p-[2-[(5-Chloro-2-methoxybenzoyl)amino]ethyl]benzenephosphonate
• CAS No.: 594854-55-4
• Molecular Formula: C₁₆H₁₇ClNO₆P
• Molecular Weight: 385.741
• Mol file: 594854-55-4.mol

Synonyms:5-Chloro-2-methoxy-N-[2-[4-(phosphonooxy)phenyl]ethyl]benzamide;p-[2-[(5-Chloro-2-methoxybenzoyl)amino]ethyl]benzenephosphonate

Chemical Property of p-[2-[(5-Chloro-2-methoxybenzoyl)amino]ethyl]benzenephosphonate

Chemical Property:

• Refractive Index: 1.603
• PKA: 1.29±0.30(Predicted)
• PSA: 111.33000
• Density: 1.431g/cm³
• LogP: 3.39140

Purity/Quality:

p-[2-[(5-Chloro-2-methoxybenzoyl)amino]ethyl]benzenephosphonate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of p-[2-[(5-Chloro-2-methoxybenzoyl)amino]ethyl]benzenephosphonate

There total 3 articles about p-[2-[(5-Chloro-2-methoxybenzoyl)amino]ethyl]benzenephosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

5-chloro-N-[2-(4-hydroxyphenyl)ethyl]-2-methoxybenzamide (41859-64-7) → {4-[2-(5-chloro-2-methoxybenzamido)ethyl]phenyl} phosphate (594854-55-4)

Guidance literature:

With trichlorophosphate;

DOI:10.1016/S0006-2952(02)01566-6

Reference yield:

tyrosamine (51-67-2) → {4-[2-(5-chloro-2-methoxybenzamido)ethyl]phenyl} phosphate (594854-55-4)

Guidance literature:

Multi-step reaction with 2 steps

1: POCl₃

With trichlorophosphate;

DOI:10.1016/S0006-2952(02)01566-6

Reference yield:

2-methoxy-5-chlorobenzoyl chloride (29568-33-0) → {4-[2-(5-chloro-2-methoxybenzamido)ethyl]phenyl} phosphate (594854-55-4)

Guidance literature:

Multi-step reaction with 2 steps

1: POCl₃

With trichlorophosphate;

DOI:10.1016/S0006-2952(02)01566-6

upstream raw materials:

5-chloro-N-[2-(4-hydroxyphenyl)ethyl]-2-methoxybenzamide

tyrosamine

2-methoxy-5-chlorobenzoyl chloride

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