1-(Cyclohex-1-en-1-yl)-2-methoxybenzene

Base Information

Chemical Name:1-(Cyclohex-1-en-1-yl)-2-methoxybenzene
CAS No.:22618-48-0
Molecular Formula:C13H16 O
Molecular Weight:188.269
Hs Code.:
NSC Number:91066
DSSTox Substance ID:DTXSID10293628
Nikkaji Number:J3.121.368A
Wikidata:Q82032501
Mol file:22618-48-0.mol

Synonyms:1-CYCLOHEXENYL-2-METHOXYBENZENE;22618-48-0;1-(cyclohex-1-en-1-yl)-2-methoxybenzene;1-(cyclohexen-1-yl)-2-methoxybenzene;NSC91066;SCHEMBL8586239;DTXSID10293628;ICCB1_000096;NSC-91066;D87892

Suppliers and Price of 1-(Cyclohex-1-en-1-yl)-2-methoxybenzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 30 raw suppliers

Chemical Property of 1-(Cyclohex-1-en-1-yl)-2-methoxybenzene

Chemical Property:

Vapor Pressure:0.00251mmHg at 25°C
Boiling Point:296.6°C at 760 mmHg
Flash Point:115.1°C
Density:1.012g/cm³
XLogP3:3.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:2
Exact Mass:188.120115130
Heavy Atom Count:14
Complexity:207

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=CC=CC=C1C2=CCCCC2

Technology Process of 1-(Cyclohex-1-en-1-yl)-2-methoxybenzene

There total 13 articles about 1-(Cyclohex-1-en-1-yl)-2-methoxybenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 79416-02-7
1-(o-methoxyphenyl)cyclohexanol

: 22618-48-0
1-(cyclohexen-1-yl)-2-methoxybenzene

Guidance literature:: With sulfuric acid; acetic acid; at 0 - 20 ℃; for 3h;
DOI:10.1002/ejoc.201801445

Reference yield: 77.0%

: 5720-06-9
2-Methoxyphenylboronic acid

: 109467-74-5
phosphoric acid cyclohex-1-enyl ester diphenyl ester

: 22618-48-0
1-(cyclohexen-1-yl)-2-methoxybenzene

Guidance literature:: With potassium phosphate; n-butyllithium; cis-[dppf]NiCl₂; In toluene; at 90 ℃; for 24h;
DOI:10.1016/S0040-4039(99)00517-1

Reference yield: 77.0%

: 22524-46-5
cyclohex-1-en-1-yl 4-methylbenzenesulfonate

: 16750-63-3
2-methoxyphenylmagnesium bromide

: 22618-48-0
1-(cyclohexen-1-yl)-2-methoxybenzene

Guidance literature:: 2-methoxyphenylmagnesium bromide; With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; 4,4,5,5-tetramethyl<1,3,2>dioxaphospholane-2-oxide; In tetrahydrofuran; at 20 ℃; for 0.0833333h; Inert atmosphere;

cyclohex-1-en-1-yl 4-methylbenzenesulfonate; In tetrahydrofuran; at 60 ℃; for 22h; chemoselective reaction; Inert atmosphere;
DOI:10.1002/chem.201002386