Benzenemethanamine, 4-fluoro-3-methoxy- (9CI)

Base Information

• Chemical Name: Benzenemethanamine, 4-fluoro-3-methoxy- (9CI)
• CAS No.: 508177-67-1
• Molecular Formula: C8H10FNO
• Molecular Weight: 155.172
• Hs Code.: 2922299090
• Mol file: 508177-67-1.mol

Synonyms:Benzenemethanamine, 4-fluoro-3-methoxy- (9CI)

Chemical Property of Benzenemethanamine, 4-fluoro-3-methoxy- (9CI)

Chemical Property:

• Boiling Point: 242.5±25.0 °C(Predicted)
• PKA: 8.98±0.10(Predicted)
• PSA: 35.25000
• Density: 1.127±0.06 g/cm3(Predicted)
• LogP: 1.99330
• Storage Temp.: Room temperature.

Purity/Quality:

97% ^*data from raw suppliers

5-Aminomethyl-2-fluoroanisole ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Benzenemethanamine, 4-fluoro-3-methoxy- (9CI)

There total 3 articles about Benzenemethanamine, 4-fluoro-3-methoxy- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

4-fluoro-3-methoxybenzonitrile (243128-37-2) → (4-fluoro-3-methoxyphenyl)methanamine (508177-67-1)

Guidance literature:

With hydrogen; acetic acid; palladium 10% on activated carbon; for 8h; under 3112.81 Torr;

Reference yield:

4-fluoro-3-methoxybenzaldehyde (128495-46-5) → (4-fluoro-3-methoxyphenyl)methanamine (508177-67-1)

Guidance literature:

4-fluoro-3-methoxybenzaldehyde; With hydroxylamine hydrochloride; sodium acetate; In ethanol; water; at 70 ℃; for 1.5h;

With palladium 10% on activated carbon; hydrogen; In methanol; ethyl acetate; for 6h; under 3040.2 Torr;

DOI:10.1039/c8md00604k

Reference yield:

→ (4-fluoro-3-methoxyphenyl)methanamine (508177-67-1)

Guidance literature:

upstream raw materials:

4-fluoro-3-methoxybenzonitrile

4-fluoro-3-methoxybenzaldehyde

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