4-Pyrimidineacetic acid, 5-amino-1,2,3,6-tetrahydro-2,6-dioxo-, ethyl ester (9CI)

Base Information

• Chemical Name: 4-Pyrimidineacetic acid, 5-amino-1,2,3,6-tetrahydro-2,6-dioxo-, ethyl ester (9CI)
• CAS No.: 467421-27-8
• Molecular Formula: C8H11N3O4
• Molecular Weight: 213.19064
• Mol file: 467421-27-8.mol

Synonyms:4-Pyrimidineacetic acid, 5-amino-1,2,3,6-tetrahydro-2,6-dioxo-, ethyl ester (9CI)

Chemical Property of 4-Pyrimidineacetic acid, 5-amino-1,2,3,6-tetrahydro-2,6-dioxo-, ethyl ester (9CI)

Chemical Property:

• PSA: 0.00000
• LogP: 0.00000

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4-Pyrimidineacetic acid, 5-amino-1,2,3,6-tetrahydro-2,6-dioxo-, ethyl ester (9CI)

There total 3 articles about 4-Pyrimidineacetic acid, 5-amino-1,2,3,6-tetrahydro-2,6-dioxo-, ethyl ester (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 36.0%

ethyl (triphenylphosphoranylidene)acetate (1099-45-2) + 6-azido-2,4(1H,3H)pyrimidinedione → 2,4-(1H,3H,6H)-6-oxo-pyrrolo[3,2-d]pyrimidinedione + ethyl 5-amino-2,4-dioxo(1H,3H)pyrimidine-6-carboxylate (467421-27-8)

Guidance literature:

In ethyl acetate; for 8h; Heating;

DOI:10.1002/hc.10048

Reference yield: 25.0%

ethyl (triphenylphosphoranylidene)acetate (1099-45-2) + 6-azido-2,4(1H,3H)pyrimidinedione → 2,4-(1H,3H,6H)-6-oxo-pyrrolo[3,2-d]pyrimidinedione + ethyl 5-amino-2,4-dioxo(1H,3H)pyrimidine-6-carboxylate (467421-27-8) + 6-oxo-7-(triphenylphosphoranylidene)-2,4-(1H,3H,5H)-6-pyrrolo[3,2-d]pyrimidinedione

Guidance literature:

In N,N-dimethyl-formamide; for 8h; Heating;

DOI:10.1002/hc.10048

Reference yield:

5-Aminouracil (932-52-5) + ethyl bromoacetate (105-36-2) → ethyl 5-amino-2,4-dioxo(1H,3H)pyrimidine-6-carboxylate (467421-27-8)

Guidance literature:

In acetonitrile; for 4h; Heating;

DOI:10.1002/hc.10048

upstream raw materials:

5-Aminouracil

ethyl bromoacetate

ethyl (triphenylphosphoranylidene)acetate

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