N,N-Dimethyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-YL)benzenesulfonamide

Base Information

Chemical Name:N,N-Dimethyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-YL)benzenesulfonamide
CAS No.:486422-05-3
Molecular Formula:C14H22BNO4S
Molecular Weight:311.21
Hs Code.:2935009090
DSSTox Substance ID:DTXSID50585953
Wikidata:Q82477975
Mol file:486422-05-3.mol

Synonyms:486422-05-3;N,N-DIMETHYL-3-(4,4,5,5-TETRAMETHYL-1,3,2-DIOXABOROLAN-2-YL)BENZENESULFONAMIDE;3-(N,N-Dimethylaminosulfonyl)phenylboronic acid pinacol ester;3-(N,N-DIMETHYLSULFAMOYL)PHENYLBORONIC ACID, PINACOL ESTER;3-(DIHYDROXYBORANE PINACOL ESTER)PHENYLDIMETHYLSULFONAMIDE;3-(N,N-Dimethylsulfamoyl)phenylboronic acid pinacol ester;SCHEMBL1674134;OSM-S-153;DTXSID50585953;MFCD07368237;AB31969;BS-23000;CS-0100023;V10169;A871900;N,N-Dimethyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzene-1-sulfonamide

Suppliers and Price of N,N-Dimethyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-YL)benzenesulfonamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
3-(N,N-Dimethylsulfamoyl)phenylboronicacid,pinacolester
100mg
$ 70.00

Crysdot
N,N-Dimethyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzenesulfonamide 95+%
5g
$ 842.00

Crysdot
N,N-Dimethyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzenesulfonamide 95+%
1g
$ 262.00

American Custom Chemicals Corporation
3-(DIHYDROXYBORANE PINACOL ESTER)PHENYLDIMETHYLSULFONAMIDE 95.00%
5MG
$ 501.72

Ambeed
N,N-Dimethyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzenesulfonamide 98%
5g
$ 403.00

Ambeed
N,N-Dimethyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzenesulfonamide 98%
250mg
$ 49.00

Ambeed
N,N-Dimethyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzenesulfonamide 98%
100mg
$ 31.00

Ambeed
N,N-Dimethyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzenesulfonamide 98%
1g
$ 121.00

Alichem
N,N-Dimethyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzenesulfonamide
1g
$ 207.05

Alichem
N,N-Dimethyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzenesulfonamide
5g
$ 748.80

Total 13 raw suppliers

Chemical Property of N,N-Dimethyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-YL)benzenesulfonamide

Chemical Property:

Boiling Point:432.1±47.0 °C(Predicted)
PKA:-4.74±0.70(Predicted)
PSA：64.22000
Density:1.18±0.1 g/cm3(Predicted)
LogP:2.31690
Storage Temp.:2-8°C
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:3
Exact Mass:311.1362595
Heavy Atom Count:21
Complexity:468

Purity/Quality:

97% ^*data from raw suppliers

3-(N,N-Dimethylsulfamoyl)phenylboronicacid,pinacolester ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:B1(OC(C(O1)(C)C)(C)C)C2=CC(=CC=C2)S(=O)(=O)N(C)C

Technology Process of N,N-Dimethyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-YL)benzenesulfonamide

There total 3 articles about N,N-Dimethyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-YL)benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 73183-34-3
bis(pinacol)diborane

: 153435-80-4
3-bromo-N,N-dimethyl-benzenesulfonamide

: 486422-05-3
N,N-dimethyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzenesulfonamide

Guidance literature:: With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sodium acetate; In 1,4-dioxane; at 80 ℃; Inert atmosphere;
DOI:10.1002/cmdc.202100018

Reference yield:

: 14417-01-7
N,N-dimethylbenzenesulfonamide

: 73183-34-3
bis(pinacol)diborane

: 486422-05-3
N,N-dimethyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzenesulfonamide

Guidance literature:: With 1,10-Phenanthroline; (1,5-cyclooctadiene)(methoxy)iridium(I) dimer; In cyclohexane; at 80 ℃; for 12h; Glovebox; Inert atmosphere;
DOI:10.1021/jacs.1c01770

Reference yield:

: 2905-24-0
3-Bromobenzenesulfonyl chloride

: 486422-05-3
N,N-dimethyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / 0 - 20 °C

2: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sodium acetate / 1,4-dioxane / 80 °C / Inert atmosphere

With pyridine; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sodium acetate; In 1,4-dioxane;
DOI:10.1002/cmdc.202100018