4-Hydrazinopyrido[3',2':4,5]thieno[3,2-d]pyrimidine

Base Information

• Chemical Name: 4-Hydrazinopyrido[3',2':4,5]thieno[3,2-d]pyrimidine
• CAS No.: 55115-84-9
• Molecular Formula: C9H7N5S
• Molecular Weight: 217.25
• Hs Code.: 2934999090
• DSSTox Substance ID: DTXSID50381477
• Wikidata: Q82172327
• Mol file: 55115-84-9.mol

Synonyms:55115-84-9;4-hydrazinopyrido[3',2':4,5]thieno[3,2-d]pyrimidine;4-HYDRAZINOPYRIDO[3',2';8-thia-3,5,10-triazatricyclo[7.4.0.02,7]trideca-1(9),2(7),3,5,10,12-hexaen-6-ylhydrazine;4-Hydrazinopyrido[3',2',4,5]thieno[3,2-d]pyrimidine;DTXSID50381477;FT-0640294

Chemical Property of 4-Hydrazinopyrido[3',2':4,5]thieno[3,2-d]pyrimidine

Chemical Property:

• Boiling Point: 517.6oC at 760 mmHg
• Flash Point: 266.8oC
• PSA: 104.96000
• Density: 1.628g/cm3
• LogP: 2.29840
• XLogP3: 1.5
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 6
• Rotatable Bond Count: 1
• Exact Mass: 217.04221642
• Heavy Atom Count: 15
• Complexity: 239

Purity/Quality:

99% ^*data from raw suppliers

4-HYDRAZINOPYRIDO[3',2':4,5]THIENO[3,2-D]PYRIMIDINE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: C1=CC2=C(N=C1)SC3=C2N=CN=C3NN

Technology Process of 4-Hydrazinopyrido[3',2':4,5]thieno[3,2-d]pyrimidine

There total 5 articles about 4-Hydrazinopyrido[3',2':4,5]thieno[3,2-d]pyrimidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-chloro-3-pyridinecarbonitrile (6602-54-6) → 4-hydrazino-pyrido[3',2':4,5]thieno[3,2-d]pyrimidine (55115-84-9)

Guidance literature:

Multi-step reaction with 5 steps

1: Na₂CO₃ / ethanol

3: POCl₃ / pyridine

4: H₂ / Pd-C / ethanol

5: N₂H₄*H₂O / ethanol

With hydrogen; sodium carbonate; hydrazine hydrate; trichlorophosphate; palladium on activated charcoal; In pyridine; ethanol;

DOI:10.1002/jhet.5570110622

Reference yield:

4-chloropyrido[3',2';4,5]thieno[3,2-d]pyrimidine (55115-80-5) → 4-hydrazino-pyrido[3',2':4,5]thieno[3,2-d]pyrimidine (55115-84-9)

Guidance literature:

Multi-step reaction with 2 steps

1: H₂ / Pd-C / ethanol

2: N₂H₄*H₂O / ethanol

With hydrogen; hydrazine hydrate; palladium on activated charcoal; In ethanol;

DOI:10.1002/jhet.5570110622

Reference yield:

Pyrido<3',2':4,5>thieno<3,2-d>pyrimidin-4(1H)-one (55115-79-2) → 4-hydrazino-pyrido[3',2':4,5]thieno[3,2-d]pyrimidine (55115-84-9)

Guidance literature:

Multi-step reaction with 3 steps

1: POCl₃ / pyridine

2: H₂ / Pd-C / ethanol

3: N₂H₄*H₂O / ethanol

With hydrogen; hydrazine hydrate; trichlorophosphate; palladium on activated charcoal; In pyridine; ethanol;

DOI:10.1002/jhet.5570110622

upstream raw materials:

pyrido[3',2':4,5]thieno[3,2-d]pyrimidine

2-chloro-3-pyridinecarbonitrile

4-chloropyrido[3',2';4,5]thieno[3,2-d]pyrimidine

Pyrido<3',2':4,5>thieno<3,2-d>pyrimidin-4(1H)-one