Technology Process of 1-(2-Hydroxy-3,5-dimethylphenyl)-3-phenylpropane-1,3-dione
There total 5 articles about 1-(2-Hydroxy-3,5-dimethylphenyl)-3-phenylpropane-1,3-dione which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
In
hexane;
for 6h;
Ambient temperature;
Irradiation;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 10 percent NaOH / 1 h / Heating
2: 57 percent / 4-dimethylaminopyridine, N,N'-dicyclohexylcarbodiimide / CHCl3 / 0.25 h / Ambient temperature
3: 87 percent / 20percent H2SO4, SiO2 / CHCl3 / 6 h
4: 13 percent / hexane / 6 h / Ambient temperature; Irradiation
With
dmap; sodium hydroxide; sulfuric acid; silica gel; dicyclohexyl-carbodiimide;
In
hexane; chloroform;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: p-toluenesulphonic acid / benzene / Heating
2: 10 percent NaOH / 1 h / Heating
3: 57 percent / 4-dimethylaminopyridine, N,N'-dicyclohexylcarbodiimide / CHCl3 / 0.25 h / Ambient temperature
4: 87 percent / 20percent H2SO4, SiO2 / CHCl3 / 6 h
5: 13 percent / hexane / 6 h / Ambient temperature; Irradiation
With
dmap; sodium hydroxide; sulfuric acid; silica gel; toluene-4-sulfonic acid; dicyclohexyl-carbodiimide;
In
hexane; chloroform; benzene;