(2,4-Dinitrophenyl)phenyl-diazene

Base Information

• Chemical Name: (2,4-Dinitrophenyl)phenyl-diazene
• CAS No.: 51640-16-5
• Molecular Formula: C12H8N4O4
• Molecular Weight: 272.22
• Hs Code.: 2927000090
• DSSTox Substance ID: DTXSID90567839
• Mol file: 51640-16-5.mol

Synonyms:51640-16-5;(2,4-DINITROPHENYL)PHENYL-DIAZENE;2,4-dinitroazobenzene;(2,4-Dinitrophenyl)phenyl diazene;DTXSID90567839;ZZGHYYQHGJJQGC-BUHFOSPRSA-N;diazene, 1-(2,4-dinitrophenyl)-2-phenyl-;(E)-1-(2,4-Dinitrophenyl)-2-phenyldiazene

Chemical Property of (2,4-Dinitrophenyl)phenyl-diazene

Chemical Property:

• Refractive Index: 1.665
• PSA: 116.36000
• LogP: 4.96480
• XLogP3: 3.4
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 6
• Rotatable Bond Count: 2
• Exact Mass: 272.05455475
• Heavy Atom Count: 20
• Complexity: 384

Purity/Quality:

99% ^*data from raw suppliers

(2,4-DINITROPHENYL)PHENYL-DIAZENE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: C1=CC=C(C=C1)N=NC2=C(C=C(C=C2)[N+](=O)[O-])[N+](=O)[O-]

Technology Process of (2,4-Dinitrophenyl)phenyl-diazene

There total 7 articles about (2,4-Dinitrophenyl)phenyl-diazene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

1-(2,4-dinitrophenyl)-2-phenylhydrazine (64264-31-9) → 1-(2,4-dinitrophenyl)-2-phenyldiazene (51640-16-5)

Guidance literature:

With hydrogenchloride; dihydrogen peroxide; acetic acid; titanium(III) chloride; hydrogen bromide; In methanol; at 20 ℃;

DOI:10.1021/ja074413c

Reference yield: 31.0%

tributylphenylstannane (960-16-7) + 2,4-dinitrophenyldiazonium tetrafluoroborate (345-12-0) → 2.4-Dinitro-azobenzol (51640-16-5)

Guidance literature:

In acetonitrile; for 18h; Ambient temperature;

Reference yield:

1-(2,4-dinitrophenyl)-2-phenylhydrazine (64264-31-9) → 2.4-Dinitro-azobenzol (51640-16-5)

Guidance literature:

With ethanol; mercury(II) oxide;

upstream raw materials:

1-(2,4-dinitrophenyl)-2-phenylhydrazine

tributylphenylstannane

2,4-dinitrophenyldiazonium tetrafluoroborate

ethanol

Downstream raw materials:

(2,4-dinitro-phenyl)-(4-nitro-phenyl)-diazene

bis-(2,4-dinitro-phenyl)-diazene

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