2-Furanmethanol, 5-ethenyltetrahydro-.alpha.,.alpha.,5-trimethyl-, acetate, cis-

Base Information

• Chemical Name: 2-Furanmethanol, 5-ethenyltetrahydro-.alpha.,.alpha.,5-trimethyl-, acetate, cis-
• CAS No.: 56469-39-7
• Molecular Formula: C12H20O3
• Molecular Weight: 212.29
• Mol file: 56469-39-7.mol

Synonyms:2-Furanmethanol, 5-ethenyltetrahydro-.alpha.,.alpha.,5-trimethyl-, acetate, cis-

Chemical Property of 2-Furanmethanol, 5-ethenyltetrahydro-.alpha.,.alpha.,5-trimethyl-, acetate, cis-

Chemical Property:

• Boiling Point: 251.4±28.0 °C(Predicted)
• Density: 1.034±0.06 g/cm3(Predicted)

Purity/Quality:

98.5% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-Furanmethanol, 5-ethenyltetrahydro-.alpha.,.alpha.,5-trimethyl-, acetate, cis-

There total 5 articles about 2-Furanmethanol, 5-ethenyltetrahydro-.alpha.,.alpha.,5-trimethyl-, acetate, cis- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

2-methyl-5-(2'-propyl-2'-hydroxy)-2-vinyltetrahydrofuran (60047-17-8,37267-80-4) + acetyl chloride (75-36-5) → acetoxy linalool oxide (56469-39-7)

Guidance literature:

With pyridine; dmap; In dichloromethane; at 0 - 20 ℃;

DOI:10.1007/BF02033674

Reference yield:

(R)-linalyl oxide (286428-24-8,37267-80-4) + acetic anhydride (108-24-7) → (2R,5S)-5-(1-acetoxy-1-methylethyl)-2-ethenyl-2-methyl-perhydrofuran (286428-30-6,56469-39-7) + (2R,5R)-5-(1-acetoxy-1-methylethyl)-2-ethenyl-2-methyl-perhydrofuran (286428-25-9,56469-39-7)

Guidance literature:

With sodium acetate; for 3h; Heating;

Reference yield:

(R)-linalyl oxide (286428-24-8,37267-80-4) + acetic anhydride (108-24-7) → (2R,5S)-5-(1-acetoxy-1-methylethyl)-2-ethenyl-2-methyl-perhydrofuran (286428-30-6,56469-39-7) + (2R,5R)-5-(1-acetoxy-1-methylethyl)-2-ethenyl-2-methyl-perhydrofuran (286428-25-9,56469-39-7)

Guidance literature:

With sodium acetate; for 3h; Heating;

upstream raw materials:

(R)-linalyl oxide

acetic anhydride

2-methyl-5-(2'-propyl-2'-hydroxy)-2-vinyltetrahydrofuran

acetyl chloride