C-(4-METHOXY-PHENYL)-C-PHENYL-METHYL-AMMONIUM CHLORIDE

Base Information

• Chemical Name: C-(4-METHOXY-PHENYL)-C-PHENYL-METHYL-AMMONIUM CHLORIDE
• CAS No.: 5267-46-9
• Molecular Formula: C14H16ClNO
• Molecular Weight: 249.74
• Hs Code.: 2922299090
• Mol file: 5267-46-9.mol

Synonyms:C-(4-METHOXY-PHENYL)-C-PHENYL-METHYLAMINE HYDROCHLORIDE;C-(4-METHOXY-PHENYL)-C-PHENYL-METHYL-AMMONIUM CHLORIDE;AKOS AU36-M298;AKOS BC-1789

Chemical Property of C-(4-METHOXY-PHENYL)-C-PHENYL-METHYL-AMMONIUM CHLORIDE

Chemical Property:

• Vapor Pressure: 5.07E-05mmHg at 25°C
• Melting Point: 190 °C
• Refractive Index: 1.581
• Boiling Point: 348.3°C at 760 mmHg
• Flash Point: 167.1°C
• PSA: 35.25000
• Density: 1.081g/cm³
• LogP: 4.24560
• Storage Temp.: Inert atmosphere,Room Temperature

Purity/Quality:

95% ^*data from raw suppliers

C-(4-METHOXY-PHENYL)-C-PHENYL-METHYL-AMMONIUM CHLORIDE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of C-(4-METHOXY-PHENYL)-C-PHENYL-METHYL-AMMONIUM CHLORIDE

There total 9 articles about C-(4-METHOXY-PHENYL)-C-PHENYL-METHYL-AMMONIUM CHLORIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

N-(diphenylmethylene)-1-(p-methoxyphenyl)-1-phenylmethanamine (69939-39-5) → 4-methoxy-benzhydrylamine; hydrochloride (5267-46-9)

Guidance literature:

With hydrogenchloride; In tetrahydrofuran; water; at 0 - 20 ℃; Inert atmosphere;

DOI:10.1039/c3sc53526f

Reference yield:

[(4-methoxy-phenyl)-phenyl-methyl]-phosphoramidic acid diethyl ester → 4-methoxy-benzhydrylamine; hydrochloride (5267-46-9)

Guidance literature:

With hydrogenchloride; water; In tetrahydrofuran; for 192h; Yield given; Ambient temperature;

DOI:10.1055/s-1999-3496

Reference yield:

bromobenzene (108-86-1,52753-63-6) → 4-methoxy-benzhydrylamine; hydrochloride (5267-46-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 1.) Mg / 1.) THF, 40-45 deg C, 2.) THF, 20-25 deg C, 2 h

2: HCl, H₂O / tetrahydrofuran / 192 h / Ambient temperature

With hydrogenchloride; water; magnesium; In tetrahydrofuran;

DOI:10.1055/s-1999-3496

upstream raw materials:

4-Methoxybenzophenone

bromobenzene

[1-(4-Methoxy-phenyl)-meth-(E)-ylidene]-phosphoramidic acid diethyl ester

1-bromo-4-methoxy-benzene