3-CHLORO-2,2-DIMETHYL-BUT-3-ENOIC ACID

Base Information

Chemical Name:3-CHLORO-2,2-DIMETHYL-BUT-3-ENOIC ACID
CAS No.:56663-75-3
Molecular Formula:C6H9ClO2
Molecular Weight:148.59
Hs Code.:2916199590

Synonyms:3-CHLORO-2,2-DIMETHYL-BUT-3-ENOIC ACID

Suppliers and Price of 3-CHLORO-2,2-DIMETHYL-BUT-3-ENOIC ACID

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
2,2-Dimethyl-3-chloro-3-butenoicAcid
10g
$ 1100.00

TRC
2,2-Dimethyl-3-chloro-3-butenoicAcid
1g
$ 140.00

ChemScene
3-chloro-2,2-dimethylbut-3-enoicacid
1g
$ 178.00

ChemScene
3-chloro-2,2-dimethylbut-3-enoicacid
250mg
$ 89.00

Biosynth Carbosynth
2,2-Dimethyl-3-chloro-3-butenoic acid
500 mg
$ 130.00

Biosynth Carbosynth
2,2-Dimethyl-3-chloro-3-butenoic acid
1 g
$ 227.20

Biosynth Carbosynth
2,2-Dimethyl-3-chloro-3-butenoic acid
2 g
$ 413.00

Biosynth Carbosynth
2,2-Dimethyl-3-chloro-3-butenoic acid
10 g
$ 1365.00

Biosynth Carbosynth
2,2-Dimethyl-3-chloro-3-butenoic acid
5 g
$ 750.80

American Custom Chemicals Corporation
3-CHLORO-2,2-DIMETHYLBUT-3-ENOIC ACID 95.00%
5MG
$ 501.84

Total 8 raw suppliers

Chemical Property of 3-CHLORO-2,2-DIMETHYL-BUT-3-ENOIC ACID

Chemical Property:

Boiling Point:218℃
PKA:2.49±0.10(Predicted)
Flash Point:86℃
PSA：37.30000
Density:1.156
LogP:1.84970

Purity/Quality:

98%Min ^*data from raw suppliers

2,2-Dimethyl-3-chloro-3-butenoicAcid ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Uses 2,2-Dimethyl-3-chloro-3-butenoic Acid (cas# 56663-75-3) is a compound useful in organic synthesis.

Technology Process of 3-CHLORO-2,2-DIMETHYL-BUT-3-ENOIC ACID

There total 5 articles about 3-CHLORO-2,2-DIMETHYL-BUT-3-ENOIC ACID which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 56663-74-2
methyl 3-chloro-2,2-dimethylbut-3-enoate

: 56663-75-3
2,2-dimethyl-3-chloro-3-butenoic acid

Guidance literature:: methyl 3-chloro-2,2-dimethylbut-3-enoate; With sodium hydroxide; water; for 5h; Heating / reflux;

With hydrogenchloride; In water;

Reference yield:

: 38923-57-8
methyl 2,2-dimethyl-3-oxobutanoate

: 56663-75-3
2,2-dimethyl-3-chloro-3-butenoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: PCl₅, DMF / CH₂Cl₂

2: NaOH / H₂O

With sodium hydroxide; phosphorus pentachloride; N,N-dimethyl-formamide; In dichloromethane; water;
DOI:10.1021/ja00850a008