3-CHLORO-2,2-DIMETHYL-BUT-3-ENOIC ACID METHYL ESTER

Base Information

Chemical Name:3-CHLORO-2,2-DIMETHYL-BUT-3-ENOIC ACID METHYL ESTER
CAS No.:56663-74-2
Molecular Formula:C₇H₁₁ClO₂
Molecular Weight:162.616
Hs Code.:2916199590
Mol file:56663-74-2.mol

Synonyms:3-CHLORO-2,2-DIMETHYL-BUT-3-ENOIC ACID METHYL ESTER

Suppliers and Price of 3-CHLORO-2,2-DIMETHYL-BUT-3-ENOIC ACID METHYL ESTER

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
Methyl3-chloro-2,2-dimethylbut-3-enoate
50mg
$ 45.00

Labseeker
3-CHLORO-2,2-DIMETHYL-BUT-3-ENOICACIDMETHYLESTER 95
10g
$ 1550.00

ChemScene
methyl3-chloro-2,2-dimethylbut-3-enoate
5g
$ 1682.00

ChemScene
methyl3-chloro-2,2-dimethylbut-3-enoate
250mg
$ 281.00

ChemScene
methyl3-chloro-2,2-dimethylbut-3-enoate
100mg
$ 169.00

ChemScene
methyl3-chloro-2,2-dimethylbut-3-enoate
1g
$ 561.00

American Custom Chemicals Corporation
3-CHLORO-2,2-DIMETHYL-BUT-3-ENOIC ACID METHYL ESTER 95.00%
5MG
$ 495.33

Total 10 raw suppliers

Chemical Property of 3-CHLORO-2,2-DIMETHYL-BUT-3-ENOIC ACID METHYL ESTER

Chemical Property:

Boiling Point:184℃
Flash Point:70℃
PSA：26.30000
Density:1.056
LogP:1.93810

Purity/Quality:

99%, ^*data from raw suppliers

Methyl3-chloro-2,2-dimethylbut-3-enoate ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 3-CHLORO-2,2-DIMETHYL-BUT-3-ENOIC ACID METHYL ESTER

There total 3 articles about 3-CHLORO-2,2-DIMETHYL-BUT-3-ENOIC ACID METHYL ESTER which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 38923-57-8
methyl 2,2-dimethyl-3-oxobutanoate

: 56663-74-2
methyl 3-chloro-2,2-dimethylbut-3-enoate

Guidance literature:: With phosphorus pentachloride; N,N-dimethyl-formamide; In dichloromethane; at 0 ℃; Reflux;

Reference yield:

: 38923-57-8
methyl 2,2-dimethyl-3-oxobutanoate

: 56663-74-2
methyl 3-chloro-2,2-dimethylbut-3-enoate

: 3,3-Dichloro-2,2-dimethyl-butyric acid methyl ester

Guidance literature:: With phosphorus pentachloride; N,N-dimethyl-formamide; In dichloromethane;
DOI:10.1021/ja00850a008

Reference yield:

: 105-45-3
acetoacetic acid methyl ester

: 56663-74-2
methyl 3-chloro-2,2-dimethylbut-3-enoate

Guidance literature:: Multi-step reaction with 2 steps

1: methyl iodide / tetrahydrofuran

2: phosphorus pentachloride / dichloromethane; N,N-dimethyl-formamide

With phosphorus pentachloride; methyl iodide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;