HEXYLDECETH-2

Base Information

• Chemical Name: HEXYLDECETH-2
• CAS No.: 52609-19-5
• Molecular Weight: 0
• Mol file: 52609-19-5.mol

Synonyms:HEXYLDECETH-2;Poly(oxy-1,2-ethanediyl), .alpha.-(2-hexyldecyl)-.omega.-hydroxy-;.alpha.-(2-hexyldexyl)-.omega.-hydroxy-Poly(oxy-1,2-ethanediyl)

Chemical Property of HEXYLDECETH-2

Chemical Property:

• Vapor Pressure: 0.051Pa at 20℃
• Boiling Point: 329℃[at 101 325 Pa]
• Density: 0.897[at 20℃]
• Water Solubility.: 9.402mg/L at 25℃

Purity/Quality:

99.9% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of HEXYLDECETH-2

There total 3 articles about HEXYLDECETH-2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-hexyldecan-1-ol (2425-77-6) + 2-(2'-(2''-Chloroethoxy)ethoxy)ethyl-2-tetrahydro-2H-pyran (85539-28-2) → 2-<2-<2-<(1-Hexyldecyl)oxy>ethoxy>ethoxy>ethanol (52609-19-5)

Guidance literature:

With n-butyllithium; pyridinium p-toluenesulfonate; Yield given. Multistep reaction; 1.) xylene, reflux, 2.) EtOH, reflux;

DOI:10.1021/jo00122a028

Reference yield:

2-hexyldecan-1-ol (2425-77-6) → 2-<2-(2-hexyldecyloxy)ethoxy>ethanol (113181-09-2,52609-19-5)

Guidance literature:

Multi-step reaction with 2 steps

1: 90 percent / pyridine / 1 h / 2 - 20 °C

2: 1.) sodium hydroxide / 1.) 15 min, 90 deg C; 2.) 18 h, 90 deg C

With pyridine; sodium hydroxide;

DOI:10.1021/j100319a032

Reference yield:

2-hexyldecyl methanesulfonate (111360-16-8) + diethylene glycol (111-46-6) → 2-<2-(2-hexyldecyloxy)ethoxy>ethanol (113181-09-2,52609-19-5)

Guidance literature:

With sodium hydroxide; Yield given. Multistep reaction; 1.) 15 min, 90 deg C; 2.) 18 h, 90 deg C;

DOI:10.1021/j100319a032

upstream raw materials:

2-hexyldecyl methanesulfonate

diethylene glycol

2-hexyldecan-1-ol

2-(2'-(2''-Chloroethoxy)ethoxy)ethyl-2-tetrahydro-2H-pyran