4,6-Diphenyl-[2,2']bipyridinyl

Base Information

• Chemical Name: 4,6-Diphenyl-[2,2']bipyridinyl
• CAS No.: 57476-59-2
• Molecular Formula: C22H16N2
• Molecular Weight: 308.382
• DSSTox Substance ID: DTXSID00403971
• Nikkaji Number: J741.251G
• Wikidata: Q82207893
• Mol file: 57476-59-2.mol

Synonyms:4,6-DIPHENYL-[2,2']BIPYRIDINYL;57476-59-2;4,6-diphenyl-2,2'-bipyridine;2,4-diphenyl-6-pyridin-2-ylpyridine;SCHEMBL6419032;DTXSID00403971;4,6-DIPHENYL-[2,2]BIPYRIDINYL;FT-0754709

Chemical Property of 4,6-Diphenyl-[2,2']bipyridinyl

Chemical Property:

• Refractive Index: 1.626
• Boiling Point: 465.7°Cat760mmHg
• Flash Point: 177.5°C
• Density: 1.134g/cm³
• XLogP3: 4.8
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 3
• Exact Mass: 308.131348519
• Heavy Atom Count: 24
• Complexity: 370

Purity/Quality:

98% ^*data from raw suppliers

4,6-DIPHENYL-2,2'-BIPYRIDINE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C(C=C1)C2=CC(=NC(=C2)C3=CC=CC=N3)C4=CC=CC=C4

Technology Process of 4,6-Diphenyl-[2,2']bipyridinyl

There total 5 articles about 4,6-Diphenyl-[2,2']bipyridinyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

2-(2-pyridyl)-4,6-diphenyl-λ3-phosphinine + [Mo(CO)4(2-(2’-pyridyl)-4,6-diphenylpyridine)] → [Mo(CO)4(2-(2’-pyridyl)-4,6-diphenylphosphinine)] + 4,6-diphenyl-[2,2']bipyridinyl (57476-59-2)

Guidance literature:

In dichloromethane; for 72h; Inert atmosphere; Schlenk technique; Glovebox; Reflux;

DOI:10.1039/c5dt01261a

Reference yield: 100.0%

2-(2-pyridyl)-4,6-diphenyl-λ3-phosphinine + [Cr(CO)4(2-(2’-pyridyl)-4,6-diphenylpyridine)] → [Cr(CO)4(2-(2’-pyridyl)-4,6-diphenylphosphinine)] + 4,6-diphenyl-[2,2']bipyridinyl (57476-59-2)

Guidance literature:

for 3h; Inert atmosphere; Schlenk technique; Glovebox; Reflux;

DOI:10.1039/c5dt01261a

Reference yield:

5-phenyl-3-(2′-pyridyl)-1,2,4-triazine (16280-66-3) + acetophenone (98-86-2) → 3,6-diphenyl-[2,2']bipyridinyl (57476-60-5) + 4,6-diphenyl-[2,2']bipyridinyl (57476-59-2)

Guidance literature:

With pyrrolidine; at 150 ℃; for 1h; microwave irradiation;

DOI:10.1021/jo0518304

upstream raw materials:

5-phenyl-3-(2′-pyridyl)-1,2,4-triazine

acetophenone

Downstream raw materials:

4,6-diphenyl-2-(N-oxido-2-pyridyl)pyridine

chloro(4,6-diphenyl-2,2'-bipyridine(-1H))platinum(II)

[Rh(I)(η4-cyclooctadiene)(2-(2'-pyridyl)-4,6-diphenylpyridine)]BF4

C₃₂H₃₁ClN₂Rh⁽¹⁺⁾*C₁₀H₁₅Cl₃Rh^(1-)

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