Carbonimidodithioic acid, 2-pyridinyl-, dimethyl ester (9CI)

Base Information

• Chemical Name: Carbonimidodithioic acid, 2-pyridinyl-, dimethyl ester (9CI)
• CAS No.: 53687-90-4
• Molecular Formula: C8H10N2S2
• Molecular Weight: 198.3084
• Mol file: 53687-90-4.mol

Synonyms:Carbonimidodithioic acid, 2-pyridinyl-, dimethyl ester (9CI)

Chemical Property of Carbonimidodithioic acid, 2-pyridinyl-, dimethyl ester (9CI)

Chemical Property:

• PSA: 75.85000
• LogP: 2.79510

Purity/Quality:

95+% ^*data from raw suppliers

Dimethylpyridin-2-ylcarbonimidodithioate 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Carbonimidodithioic acid, 2-pyridinyl-, dimethyl ester (9CI)

There total 2 articles about Carbonimidodithioic acid, 2-pyridinyl-, dimethyl ester (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

pyridin-2-yl-dithiocarbamic acid methyl ester (13037-46-2) + methyl iodide (74-88-4) → dimethyl N-(2-pyridyl)dithiocarbonimidate (53687-90-4)

Guidance literature:

With ethanol; sodium ethanolate;

DOI:10.1039/jr9560001644

Reference yield:

2-aminopyridine (504-29-0) + carbon disulfide (75-15-0,12122-00-8) + methyl iodide (74-88-4) → dimethyl N-(2-pyridyl)dithiocarbonimidate (53687-90-4)

Guidance literature:

With sodium hydroxide; Multistep reaction; 1.) RT, 0.5 h, 2.) 0 deg C, 2 h;

upstream raw materials:

pyridin-2-yl-dithiocarbamic acid methyl ester

methyl iodide

2-aminopyridine

carbon disulfide

Refernces