Methyl 2-pyridinyldithiocarbamate

Base Information

Chemical Name:Methyl 2-pyridinyldithiocarbamate
CAS No.:13037-46-2
Molecular Formula:C7H8 N2 S2
Molecular Weight:184.286
Hs Code.:
DSSTox Substance ID:DTXSID10418637
Nikkaji Number:J261.946F
Mol file:13037-46-2.mol

Synonyms:Methyl 2-pyridinyldithiocarbamate;13037-46-2;methyl N-pyridin-2-ylcarbamodithioate;Carbamodithioic acid, N-2-pyridinyl-, methyl ester;Methyl 2-pyridyldithiocarbamate;methyl pyridin-2-ylcarbamodithioate;methyl-2-pyridyldithiocarbamate;SCHEMBL8691428;DTXSID10418637;Methyl 2-pyridinyldithiocarbamate #;AKOS000269366;N-(2-Pyridyl)dithiocarbamic acid methyl ester;N-(pyridin-2-yl)(methylsulfanyl)carbothioamide

Suppliers and Price of Methyl 2-pyridinyldithiocarbamate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of Methyl 2-pyridinyldithiocarbamate

Chemical Property:

Melting Point:91 °C(Solv: ethanol (64-17-5))
Boiling Point:303.1±34.0 °C(Predicted)
PKA:9.99±0.70(Predicted)
PSA：89.35000
Density:1.339±0.06 g/cm3(Predicted)
LogP:2.36190
XLogP3:2.2
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:2
Exact Mass:184.01289061
Heavy Atom Count:11
Complexity:138

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CSC(=S)NC1=CC=CC=N1

Technology Process of Methyl 2-pyridinyldithiocarbamate

There total 8 articles about Methyl 2-pyridinyldithiocarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 504-29-0
2-aminopyridine

: 75-15-0,12122-00-8
carbon disulfide

: 74-88-4
methyl iodide

: 13037-46-2
pyridin-2-yl-dithiocarbamic acid methyl ester

Guidance literature:: 2-aminopyridine; carbon disulfide; With potassium hydroxide; In dimethyl sulfoxide;

methyl iodide; In dimethyl sulfoxide; at 20 ℃;
DOI:10.1016/j.bmcl.2004.02.079

Reference yield:

: 504-29-0
2-aminopyridine

: 75-15-0,12122-00-8
carbon disulfide

: 77-78-1
dimethyl sulfate

: 13037-46-2
pyridin-2-yl-dithiocarbamic acid methyl ester

Guidance literature:: 2-aminopyridine; carbon disulfide; With sodium hydroxide; In dimethyl sulfoxide; for 0.5h;

dimethyl sulfate; In water; dimethyl sulfoxide; for 2h; Further stages.; cooling;

Reference yield:

: 504-29-0
2-aminopyridine

: 13037-46-2
pyridin-2-yl-dithiocarbamic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N / 2 h / Heating

2: CH₂Cl₂ / 0 °C

With triethylamine; In dichloromethane;
DOI:10.1021/ja952591c