1-Propanol,2-[[(4-methoxyphenyl)methylene]amino]-,(2R)-(9CI)

Base Information

Chemical Name:1-Propanol,2-[[(4-methoxyphenyl)methylene]amino]-,(2R)-(9CI)
CAS No.:697763-78-3
Molecular Formula:C11H15 N O2
Molecular Weight:193.246
Hs Code.:
Mol file:697763-78-3.mol

Synonyms:1-Propanol,2-[[(4-methoxyphenyl)methylene]amino]-,(2R)-(9CI)

Suppliers and Price of 1-Propanol,2-[[(4-methoxyphenyl)methylene]amino]-,(2R)-(9CI)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-Propanol,2-[[(4-methoxyphenyl)methylene]amino]-,(2R)-(9CI)

Chemical Property:

PSA：41.82000
LogP:1.49490

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1-Propanol,2-[[(4-methoxyphenyl)methylene]amino]-,(2R)-(9CI)

There total 1 articles about 1-Propanol,2-[[(4-methoxyphenyl)methylene]amino]-,(2R)-(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 35320-23-1
(R)-2-aminopropan-1-ol

: 123-11-5
4-methoxy-benzaldehyde

: 697763-78-3
C₁₁H₁₅NO₂

Guidance literature:: In toluene; at 50 ℃; for 72h; Molecular sieve; Inert atmosphere;
DOI:10.2174/157017810791514814

Reference yield: 100.0%

: 697763-78-3
C₁₁H₁₅NO₂

: 570398-17-3
(R)-2-((4-methoxybenzyl)amino)propan-1-ol

Guidance literature:: With sodium tetrahydroborate; In methanol; at 25 ℃; for 1h;

Reference yield:

: 697763-78-3
C₁₁H₁₅NO₂

: C₂₁H₂₂N₄O₃

Guidance literature:: Multi-step reaction with 7 steps

1.1: sodium tetrahydroborate / methanol / 1 h / 25 °C

2.1: N-ethyl-N,N-diisopropylamine; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate / N,N-dimethyl-formamide / 18 h / 20 °C

3.1: potassium phosphate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene / tetrahydrofuran / 0.17 h / 20 °C / Inert atmosphere

3.2: 3.17 h / 20 - 90 °C / Inert atmosphere

4.1: hydrogenchloride / methanol; isopropyl alcohol / 20 °C

5.1: acetic anhydride / 0.5 h / 20 °C

5.2: 16 h / 60 °C

6.1: potassium carbonate; potassium iodide / N,N-dimethyl-formamide / 16 h / 20 °C

7.1: ammonium acetate / acetic acid / 1 h / Reflux

With hydrogenchloride; sodium tetrahydroborate; potassium phosphate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; ammonium acetate; acetic anhydride; potassium carbonate; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; potassium iodide; In tetrahydrofuran; methanol; acetic acid; N,N-dimethyl-formamide; isopropyl alcohol;