1H-Pyrrole-2-carboxaldehyde, 1-(2-methyl-2-propenyl)- (9CI)

Base Information

Chemical Name:1H-Pyrrole-2-carboxaldehyde, 1-(2-methyl-2-propenyl)- (9CI)
CAS No.:631869-23-3
Molecular Formula:C9H11NO
Molecular Weight:149.18974
Hs Code.:
Mol file:631869-23-3.mol

Synonyms:1H-Pyrrole-2-carboxaldehyde, 1-(2-methyl-2-propenyl)- (9CI)

Suppliers and Price of 1H-Pyrrole-2-carboxaldehyde, 1-(2-methyl-2-propenyl)- (9CI)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1H-Pyrrole-2-carboxaldehyde, 1-(2-methyl-2-propenyl)- (9CI)

Chemical Property:

Boiling Point:30 °C(Press: 0.2 Torr)
PKA:-7.35±0.70(Predicted)
PSA：22.00000
Density:0.96±0.1 g/cm3(Predicted)
LogP:1.87670

Purity/Quality:

Safty Information:

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Hazard Codes:

MSDS Files:

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Technology Process of 1H-Pyrrole-2-carboxaldehyde, 1-(2-methyl-2-propenyl)- (9CI)

There total 4 articles about 1H-Pyrrole-2-carboxaldehyde, 1-(2-methyl-2-propenyl)- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1003-29-8,254729-95-8
2-pyrrole aldehyde

: 563-47-3
3-Chloro-2-methylpropene

: 631869-23-3
1-(2-methylprop-2-enyl)pyrrole-2-carbaldehyde

Guidance literature:: With sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate; In toluene; at 70 ℃; for 1h;
DOI:10.1081/SCC-120022467

Reference yield: 71.0%

: 1003-29-8,254729-95-8
2-pyrrole aldehyde

: 513-37-1
2-methylprop-1-enyl chloride

: 631869-23-3
1-(2-methylprop-2-enyl)pyrrole-2-carbaldehyde

Guidance literature:: 2-pyrrole aldehyde; With 18-crown-6 ether; potassium hydroxide; In benzene; for 2h; Reflux;

2-methylprop-1-enyl chloride; In benzene; for 6h; Reflux;
DOI:10.1021/jo300779q

Reference yield: 70.0%

: 1003-29-8,254729-95-8
2-pyrrole aldehyde

: 1458-98-6
2-methyl-3-bromo-1-propene

: 631869-23-3
1-(2-methylprop-2-enyl)pyrrole-2-carbaldehyde

Guidance literature:: 2-pyrrole aldehyde; With caesium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 0.5h; Inert atmosphere;

2-methyl-3-bromo-1-propene; In N,N-dimethyl-formamide; at 20 ℃; Inert atmosphere;
DOI:10.1021/ol501869s