Cyclopentanecarboxamide, N-(1,3,4,6,7,8-hexahydro-6,8-dioxo-7-propyl-2H-pyrimido[1,6-a]pyrimidin-9-yl)-

Base Information

Chemical Name:Cyclopentanecarboxamide, N-(1,3,4,6,7,8-hexahydro-6,8-dioxo-7-propyl-2H-pyrimido[1,6-a]pyrimidin-9-yl)-
CAS No.:524944-76-1
Molecular Formula:C16H24N4O3
Molecular Weight:320.39
Hs Code.:
Mol file:524944-76-1.mol

Synonyms:Cyclopentanecarboxamide, N-(1,3,4,6,7,8-hexahydro-6,8-dioxo-7-propyl-2H-pyrimido[1,6-a]pyrimidin-9-yl)-

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Cyclopentanecarboxamide, N-(1,3,4,6,7,8-hexahydro-6,8-dioxo-7-propyl-2H-pyrimido[1,6-a]pyrimidin-9-yl)-

Chemical Property:

Melting Point:179 °C
PSA：85.13000
LogP:1.57530

Purity/Quality:

Safty Information:

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Technology Process of Cyclopentanecarboxamide, N-(1,3,4,6,7,8-hexahydro-6,8-dioxo-7-propyl-2H-pyrimido[1,6-a]pyrimidin-9-yl)-

There total 3 articles about Cyclopentanecarboxamide, N-(1,3,4,6,7,8-hexahydro-6,8-dioxo-7-propyl-2H-pyrimido[1,6-a]pyrimidin-9-yl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 109-64-8
1,3-dibromo-propane

: 152529-70-9
Cyclopentane carboxylic acid (6-amino-2,4-dioxo-3-propyl-1,2,3,4-tetra hydro-pyrimidin-5-yl)-amide

: 524944-76-1
9-cyclopentanecarboxamido-6,8-dioxo-7-propyl-1,3,4,6,7,8-hexahydro-2H-pyrimido[1,6-a]pyrimidine

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 60 ℃; for 2h;
DOI:10.1016/S0040-4020(02)01485-0

Reference yield:

: 3400-45-1
cyclopentanecarboxylic acid

: 524944-76-1
9-cyclopentanecarboxamido-6,8-dioxo-7-propyl-1,3,4,6,7,8-hexahydro-2H-pyrimido[1,6-a]pyrimidine

Guidance literature:: Multi-step reaction with 2 steps

1: 60 percent / N'-(3-dimethylaminopropyl)-N-ethylcarbodiimide hydrochloride / methanol / 3 h / 20 °C

2: 56 percent / K₂CO₃ / dimethylformamide / 2 h / 60 °C

With potassium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In methanol; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(02)01485-0

Reference yield:

: 142665-13-2
5,6-diamino-3-propyluracil

: 524944-76-1
9-cyclopentanecarboxamido-6,8-dioxo-7-propyl-1,3,4,6,7,8-hexahydro-2H-pyrimido[1,6-a]pyrimidine

Guidance literature:: Multi-step reaction with 2 steps

1: 60 percent / N'-(3-dimethylaminopropyl)-N-ethylcarbodiimide hydrochloride / methanol / 3 h / 20 °C

2: 56 percent / K₂CO₃ / dimethylformamide / 2 h / 60 °C

With potassium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In methanol; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(02)01485-0