IRON(II) 1,2,3,4,8,9,10,11,15,16,17,18,22,23,24,25-HEXADECACHLORO-29 H,31 H-PHTHALOCYANINE

Base Information

Chemical Name:IRON(II) 1,2,3,4,8,9,10,11,15,16,17,18,22,23,24,25-HEXADECACHLORO-29 H,31 H-PHTHALOCYANINE
CAS No.:50662-67-4
Molecular Formula:C₃₂Cl₁₆FeN₈
Molecular Weight:1119.5
Hs Code.:

Synonyms:IRON(II) 1,2,3,4,8,9,10,11,15,16,17,18,22,23,24,25-HEXADECACHLORO-29 H,31 H-PHTHALOCYANINE;iron(ii) 1,2,3,4,8,9,10,11,15,16,17,18,22;IRON(II) 1,2,3,4,8,9,10,11,15,16,17,18,2 2, 23,24,25-HEXADECACHLORO-PHTHALOCYANI

Suppliers and Price of IRON(II) 1,2,3,4,8,9,10,11,15,16,17,18,22,23,24,25-HEXADECACHLORO-29 H,31 H-PHTHALOCYANINE

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
IRON(II)-1,2,3,4,8,9,10,11,15,16,17,18,22,23,24,25-HEXADECACHLORO-29H,31H-PHTHALOCYANINE 95.00%
5MG
$ 499.59

Total 1 raw suppliers

Chemical Property of IRON(II) 1,2,3,4,8,9,10,11,15,16,17,18,22,23,24,25-HEXADECACHLORO-29 H,31 H-PHTHALOCYANINE

Chemical Property:

Melting Point:>300 °C(lit.)
PSA：105.48000
LogP:19.16170

Purity/Quality:

≥95% ^*data from raw suppliers

IRON(II)-1,2,3,4,8,9,10,11,15,16,17,18,22,23,24,25-HEXADECACHLORO-29H,31H-PHTHALOCYANINE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

Technology Process of IRON(II) 1,2,3,4,8,9,10,11,15,16,17,18,22,23,24,25-HEXADECACHLORO-29 H,31 H-PHTHALOCYANINE

There total 1 articles about IRON(II) 1,2,3,4,8,9,10,11,15,16,17,18,22,23,24,25-HEXADECACHLORO-29 H,31 H-PHTHALOCYANINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: iron(II) chloride tetrahydrate

: 117-08-8
tetrachlorophthalic anhydride

: 50662-67-4
iron(II) 1,2,3,4,8,9,10,11,15,16,17,18,22,23,24,25=hexadecachloro-29H,31H-phthalocyanine

Guidance literature:: With ammonium molybdate; urea; In nitrobenzene; byproducts: ammonia; urea, ligand, FeCl2*4H2O, ammonium molybdate were pulverized and stirred into nitrobenzene, suspn. was heated to 180-190°C for 0.5 h, maintatined for 4 h, cooled to 90°C, diluted with EtOH; filtered hot, residue was washed with boiling H2O, ppt. was boiled for 10 min each in HCl and NaOH, extd. with chlorobenzene for 3 d; elem. anal.;

Reference yield: 54.0%

: 50662-67-4
iron(II) 1,2,3,4,8,9,10,11,15,16,17,18,22,23,24,25=hexadecachloro-29H,31H-phthalocyanine

: 110-54-3
hexane

: 21050-13-5
bis(triphenylphosphine)iminium chloride

: 95-50-1
1,2-dichloro-benzene

: (PPN)[(Fe^ICl₁₆Pc)]*0.78C₆H₄Cl₂*0.22C₆H₁₄

Guidance literature:: iron(II) 1,2,3,4,8,9,10,11,15,16,17,18,22,23,24,25=hexadecachloro-29H,31H-phthalocyanine; bis(triphenylphosphine)iminium chloride; 1,2-dichloro-benzene; With fluorenone radical anion sodium contact ion pair; at 100 ℃; for 2h; Glovebox;

hexane; Glovebox;
DOI:10.1002/ejic.201400126

Reference yield: 54.0%

: 128590-38-5
sodium fluorenone ketyl

: 50662-67-4
iron(II) 1,2,3,4,8,9,10,11,15,16,17,18,22,23,24,25=hexadecachloro-29H,31H-phthalocyanine

: 110-54-3
hexane

: 21050-13-5
bis(triphenylphosphine)iminium chloride

: 95-50-1
1,2-dichloro-benzene

: C₃₂Cl₁₆FeN₈^(1-)*0.78C₆H₄Cl₂*0.22C₆H₁₄*C₃₆H₃₀NP₂⁽¹⁺⁾

Guidance literature:: sodium fluorenone ketyl; iron(II) 1,2,3,4,8,9,10,11,15,16,17,18,22,23,24,25=hexadecachloro-29H,31H-phthalocyanine; bis(triphenylphosphine)iminium chloride; 1,2-dichloro-benzene; at 100 ℃; for 2h;

hexane;
DOI:10.1002/ejic.201400126