Ethanone, 1-(4-ethyl-2-pyridinyl)- (9CI)

Base Information

Chemical Name:Ethanone, 1-(4-ethyl-2-pyridinyl)- (9CI)
CAS No.:59576-27-1
Molecular Formula:C9H11NO
Molecular Weight:149.18974
Hs Code.:
Mol file:59576-27-1.mol

Synonyms:Ethanone, 1-(4-ethyl-2-pyridinyl)- (9CI)

Suppliers and Price of Ethanone, 1-(4-ethyl-2-pyridinyl)- (9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of Ethanone, 1-(4-ethyl-2-pyridinyl)- (9CI)

Chemical Property:

Boiling Point:100 - 101 °C (11 mmHg)
PSA：29.96000
LogP:1.84660

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Ethanone, 1-(4-ethyl-2-pyridinyl)- (9CI)

There total 5 articles about Ethanone, 1-(4-ethyl-2-pyridinyl)- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 127-19-5,116057-81-9
N,N-dimethyl acetamide

: 54453-91-7
2-bromo-4-ethylpyridine

: 59576-27-1
2-acetyl-4-ethylpyridine

Guidance literature:: With n-butyllithium; In diethyl ether; hexane;
DOI:10.1021/ja9623626

Reference yield:

: 92486-38-9
2-cyano-4-ethylpyridine

: 917-64-6
methyl magnesium iodide

: 59576-27-1
2-acetyl-4-ethylpyridine

Guidance literature:: With diethyl ether; benzene; Und folgenden Hydrolisieren;
DOI:10.1021/ja01603a036

Reference yield:

: 536-75-4,151103-55-8
4-Ethylpyridine

: 59576-27-1
2-acetyl-4-ethylpyridine

Guidance literature:: Multi-step reaction with 4 steps

1: NaNH₂; N,N-dimethyl-aniline / 130 - 140 °C

2: bromine; aqueous sodium nitrite solution; aqueous hydrobromic acid

3: zuletzt unter vermindertem Druck

4: diethyl ether; benzene / Und folgenden Hydrolisieren

With diethyl ether; hydrogen bromide; bromine; sodium amide; N,N-dimethyl-aniline; sodium nitrite; benzene;
DOI:10.1021/ja01603a036